Yancey E M, Lien W, Nuttall C S, Brewster J A, Roberts H W, Vandewalle K S
Oper Dent. 2019 Jan/Feb;44(1):34-41. doi: 10.2341/17-304-L. Epub 2018 Apr 9.
A new nanofiber-reinforced hybrid composite (NovaPro Fill, Nanova) was recently introduced with reportedly improved mechanical properties. The purpose of this study was to compare the properties (flexural strength/modulus, degree of conversion [DC], depth of cure, and polymerization shrinkage) of the nanofiber composite to those of traditional hybrid composites (Filtek Z250, 3M ESPE; Esthet-X HD, Dentsply). To determine flexural strength and modulus, composite was placed in a rectangular mold, light-cured, stored for 24 hours, and then fractured in a universal testing machine. For degree of conversion, composite was placed in a cylindrical mold, light-cured, and stored for 24 hours. Measurements were made at the top and bottom surfaces using Fourier Transform Infrared Spectroscopy. To determine depth of cure, composite was placed in a cylindrical mold and light-cured. Uncured composite was scraped until polymerized resin was reached. Remaining composite was measured and divided by two. Polymerization shrinkage was determined by placing the composite material on a pedestal in a video-imaging device while light-curing. Shrinkage was determined after 10 minutes. Data were analyzed with one-way analysis of variance and Tukey post hoc test per property (α=0.05). Compared to Filtek Z250, NovaPro Fill had significantly lower flexural strength and modulus, greater volumetric shrinkage, and similar depth of cure, but greater top and bottom DC. Compared to Esthet-X HD, NovaPro Fill had similar flexural strength, shrinkage, and top and bottom DC, but significantly greater depth of cure and flexural modulus.
最近推出了一种新型纳米纤维增强混合复合材料(NovaPro Fill,Nanova),据报道其机械性能有所改善。本研究的目的是比较纳米纤维复合材料与传统混合复合材料(Filtek Z250,3M ESPE;Esthet-X HD,Dentsply)的性能(弯曲强度/模量、转化率[DC]、固化深度和聚合收缩率)。为了测定弯曲强度和模量,将复合材料置于矩形模具中,光固化,储存24小时,然后在万能试验机中折断。对于转化率,将复合材料置于圆柱形模具中,光固化,并储存24小时。使用傅里叶变换红外光谱法在顶面和底面进行测量。为了测定固化深度,将复合材料置于圆柱形模具中并光固化。刮去未固化的复合材料,直到达到聚合树脂。测量剩余的复合材料并除以二。通过在视频成像设备中光固化时将复合材料放置在基座上来测定聚合收缩率。10分钟后测定收缩率。对每个性能的数据进行单因素方差分析和Tukey事后检验(α=0.05)。与Filtek Z2S0相比,NovaPro Fill的弯曲强度和模量显著更低,体积收缩率更大,固化深度相似,但顶面和底面的DC更高。与Esthet-X HD相比,NovaPro Fill的弯曲强度、收缩率以及顶面和底面的DC相似,但固化深度和弯曲模量显著更大。