Al Rifaiy Mohammed Qasim
Mohammed Q. Al Rifaiy, Department of Prosthetic Dental Sciences, College of Dentistry, King Saud University, Riyadh 11545, P.O. Box: 60169, Saudi Arabia.
Pak J Med Sci. 2018 Jan-Feb;34(1):32-36. doi: 10.12669/pjms.341.13916.
To assess the bond strength of LD ceramics with resin composite material and surface conditioning using Er: YSGG laser and HF acid.
Thirty LD ceramic (Emax, Ivoclar vivadent) discs were prepared using hot pressing technique and treated with hydroflouric acid (Group-1-HF acid) (9%) (n=10) and Er- yttrium, scandium, gallium and garnet laser (Group-2-ER-YSGG laser) (Waterlase iPlus, 10 Hz and power of 0.5 W, pulse duration of 230 μs) (n=10). Ten specimens were left untreated to be included as controls (Group-3-Control). All the specimens were treated with Adper Single Bond adhesive (3MESPE, St. Paul, MN, USA). Multicore buildups (3mmx3mm) were performed using a rubber mold on the ceramic surfaces and cured using LED light-curing unit for 140 sec. All specimens were tested using shear bond test and failure modes were assessed with a stereomicroscope and scanning electron microscope. Data was analysed using ANOVA and Tukey Kramer multiple comparisons test.
The maximum and minimum shear bond strength values were achieved in HF Acid specimens (Group-1) (28.15±4.72 MPa) and control specimens (13.47± 3.14 MPa) respectively. Specimens treated with HF acid showed significantly higher bond strength in comparison to laser treated and control specimens (p<0.01). Laser treated specimens had significantly higher bond strength as compared to controls (p<0.01).
Hydrofluoric (HF) acid treatment showed significantly better outcomes than YSGG laser surface treatment.
评估镧系双掺杂(LD)陶瓷与树脂复合材料的粘结强度,以及使用铒:钇钪镓石榴石(Er: YSGG)激光和氢氟酸进行表面处理的效果。
采用热压技术制备30个LD陶瓷(义获嘉威兰德公司的Emax)圆盘,并分别用氢氟酸(第1组 - 氢氟酸)(9%)(n = 10)和铒 - 钇、钪、镓和石榴石激光(第2组 - Er - YSGG激光)(Waterlase iPlus,10 Hz,功率0.5 W,脉冲持续时间230 μs)(n = 10)进行处理。10个样本未作处理作为对照(第3组 - 对照)。所有样本均用Adper单组分粘结剂(美国明尼苏达州圣保罗市3M公司)处理。在陶瓷表面使用橡胶模具进行多层堆积(3mm×3mm),并使用LED光固化机固化140秒。所有样本均采用剪切粘结试验进行测试,并通过体视显微镜和扫描电子显微镜评估破坏模式。使用方差分析和Tukey Kramer多重比较检验对数据进行分析。
氢氟酸处理的样本(第1组)获得了最大和最小剪切粘结强度值,分别为(28.15±4.72 MPa)和对照样本(13.47±3.14 MPa)。与激光处理和对照样本相比,经氢氟酸处理的样本显示出显著更高的粘结强度(p<0.01)。与对照相比,激光处理的样本具有显著更高的粘结强度(p<0.01)。
氢氟酸(HF)处理显示出比YSGG激光表面处理显著更好的效果。