Su Qian, Xu Jie, Li Yuqiao, Yoon Jae Ik, Shan Debin, Guo Bin, Kim Hyoung Seop
Key Laboratory of Micro-Systems and Micro-Structures Manufacturing of Ministry of Education, Harbin Institute of Technology, Harbin 150080, China.
School of Materials Science and Engineering, Harbin Institute of Technology, Harbin 150001, China.
Materials (Basel). 2018 Apr 13;11(4):598. doi: 10.3390/ma11040598.
Microstructural evolution and mechanical properties of LZ91 Mg-Li alloy processed by high-pressure torsion (HPT) at an ambient temperature were researched in this paper. The microstructure analysis demonstrated that significant grain refinement was achieved after HPT processing with an average grain size reducing from 30 μm (the as-received condition) to approximately 230 nm through 10 turns. X-ray diffraction analysis revealed LZ91 alloy was consisted of α phase (hexagonal close-packed structure, hcp) and β phase (body-centered cubic structure, bcc) before and after HPT processing. The mean value of microhardness increased with the increasing number of HPT turns. This significantly increased hardness of specimens can be explained by Hall-Petch strengthening. Simultaneously, the distribution of microhardness along the specimens was different from other materials after HPT processing due to the different mechanical properties of two different phases. The mechanical properties of LZ91 alloy processed by HPT were assessed by the micro-tensile testing at 298, 373, 423, and 473 K. The results demonstrate that the ultra-fine grain LZ91 Mg-Li alloy exhibits excellent mechanical properties: tensile elongation is approximately 400% at 473 K with an initial strain rate of 1 × 10 s.
本文研究了室温下通过高压扭转(HPT)加工的LZ91镁锂合金的微观结构演变和力学性能。微观结构分析表明,经过HPT加工后实现了显著的晶粒细化,平均晶粒尺寸从30μm(初始状态)通过10次扭转减小到约230nm。X射线衍射分析表明,HPT加工前后LZ91合金均由α相(六方密堆积结构,hcp)和β相(体心立方结构,bcc)组成。显微硬度平均值随HPT扭转次数的增加而增加。这种显著提高的试样硬度可以用霍尔-佩奇强化来解释。同时,由于两种不同相的力学性能不同,HPT加工后试样沿长度方向的显微硬度分布与其他材料不同。通过在298、373、423和473K下进行微拉伸试验,评估了HPT加工的LZ91合金的力学性能。结果表明,超细晶粒LZ91镁锂合金具有优异的力学性能:在473K、初始应变速率为1×10 s时,拉伸伸长率约为400%。