Akporiaye Duncan E, Dahl Ivar M, Karlsson Arne, Wendelbo Rune
Sintef Applied Chemistry, P. O. BOX 124, Blindern, N-0314 Oslo (Norway), Fax: (+47) 2206-7350.
Angew Chem Int Ed Engl. 1998 Mar 16;37(5):609-611. doi: 10.1002/(SICI)1521-3773(19980316)37:5<609::AID-ANIE609>3.0.CO;2-X.
One hundred or more solid-state syntheses can be conducted in parallel and employed for the combinatorial hydrothermal syntheses of zeolites by using a novel multiautoclave design. The operation of the multiautoclave was ascertained by the reinvestigation of the complete Na O-Al O -SiO ternary system in a single experiment. In the picture on the right, the shaded areas on the left show the crystallization fields of the different phases obtained.
通过使用一种新型的多釜设计，可以并行进行一百次或更多的固态合成，并将其用于沸石的组合水热合成。通过在单个实验中对完整的Na₂O-Al₂O₃-SiO₂三元体系进行重新研究，确定了多釜的运行情况。在右图中，左侧的阴影区域显示了所获得的不同相的结晶区域。
