School of Health Sciences, Dentistry Department, Aristotle University of Thessaloniki, Thessaloniki 54124, Greece.
Physics Department, Aristotle University of Thessaloniki, Thessaloniki 54124, Greece.
J Mech Behav Biomed Mater. 2018 Oct;86:77-83. doi: 10.1016/j.jmbbm.2018.06.019. Epub 2018 Jun 26.
The aim of this study was to evaluate microhardness and elastic modulus of a novel sol-gel derived dental ceramic - 58S bioactive glass composite (BP67: Bioactive Glass:33.3%, Dental Ceramic:66.7%) BP67 material by micro-indentation and to investigate its microstructure and bioactivity. The research hypotheses were that the values of microhardness (1) and elastic modulus (2) of the novel bioceramic composite and the commercial dental ceramic will be of the same order. The experimental sol-gel derived ceramics showed similar microstructural characteristics to a commercial feldspathic porcelain, and presence of additional calcium phosphate phases, which contributed its bioactivity. The formation of an apatite-like layer on the materials' surface observed by Fourier Transform Infrared (FTIR) spectroscopy, X-ray Diffraction (XRD) and Scanning Electron Microscopy-Energy Dispersive Spectroscopy (SEM-EDS) techniques after 12 days of maintenance in Conventional Simulated Body Fluid (cSBF) solution. The BP67 exhibited values of microhardness and modulus of elasticity which were not statistically significant different compared to dental ceramic, indicating the adequate mechanical integrity of the material. The results of this study suggest that the novel bioactive composite could be potentially applied in prosthetic dentistry, while its thermal and optical properties should be investigated in future studies.
本研究旨在通过微压痕评估新型溶胶-凝胶衍生牙科陶瓷-58S 生物活性玻璃复合材料(BP67:生物活性玻璃:33.3%,牙科陶瓷:66.7%)BP67 材料的显微硬度和弹性模量,并研究其微观结构和生物活性。研究假设为新型生物陶瓷复合材料和商业牙科陶瓷的显微硬度值(1)和弹性模量值(2)将处于同一数量级。实验溶胶-凝胶衍生陶瓷表现出与商业长石质瓷相似的微观结构特征,并存在额外的磷酸钙相,这使其具有生物活性。通过傅里叶变换红外(FTIR)光谱、X 射线衍射(XRD)和扫描电子显微镜-能量色散光谱(SEM-EDS)技术观察到材料表面形成了类似于磷灰石的层,在常规模拟体液(cSBF)溶液中保持 12 天后。BP67 的显微硬度和弹性模量值与牙科陶瓷相比无统计学差异,表明材料具有足够的机械完整性。本研究结果表明,新型生物活性复合材料可能有潜力应用于修复牙科领域,但其热学和光学性能应在未来的研究中进行研究。