Lalithamba Haraluru Shankraiah, Raghavendra Mahadevaiah, Uma Kogali, Yatish Kalanakoppal Venkatesh, Mousumi Das, Nagendra Govindappa
Acta Chim Slov. 2018 Jun;65(2):354-364. doi: 10.17344/acsi.2017.4034.
A simple, efficient and convenient method for the preparation of zinc oxide (ZnO) nanoparticle was described. Several parameters like size and morphology of the prepared nanoparticles were characterized thorough a variety of analytical techniques such as XRD, FT-IR, UV-Vis, SEM, and EDX. The prepared ZnO nanoparticles were successfully used as catalyst for the formylation of amino acid esters and biodiesel synthesis. Further, the synthesized formamide esters were well characterized through HRMS, 1H NMR and 13C NMR analysis and subjected for the in vitro antibacterial and antifungal tests and the results indicated that some of them showed promising activity against targeted bacterial pathogens.
描述了一种制备氧化锌(ZnO)纳米颗粒的简单、高效且便捷的方法。通过多种分析技术,如XRD、FT-IR、UV-Vis、SEM和EDX,对制备的纳米颗粒的尺寸和形态等几个参数进行了表征。制备的ZnO纳米颗粒成功用作氨基酸酯甲酰化和生物柴油合成的催化剂。此外,通过HRMS、1H NMR和13C NMR分析对合成的甲酰胺酯进行了充分表征,并进行了体外抗菌和抗真菌测试,结果表明其中一些对靶向细菌病原体显示出有前景的活性。