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使用硅胶进行呼气乙醇收集的长期实地经验。

A long-term field experience with breath ethanol collection employing silica gel.

作者信息

Goldberger B A, Caplan Y H, Zettl J R

出版信息

J Anal Toxicol. 1986 Sep-Oct;10(5):194-7. doi: 10.1093/jat/10.5.194.

DOI:10.1093/jat/10.5.194
PMID:3022069
Abstract

Breath specimens (N = 143) from human subjects initially analyzed for ethanol content by infrared spectroscopy were collected onto silica gel. The specimens were retained 1.25 to 2.75 years following adsorption and subsequently analyzed by headspace gas chromatography. The results revealed good overall correlation between the direct and delayed ethanol determinations (r = 0.900). Specimens were collected by police officers following a defined protocol and the results are presented to illustrate practical use and limitations of such a technique.

摘要

对最初通过红外光谱法分析乙醇含量的人体受试者的呼气样本(N = 143)收集到硅胶上。样本在吸附后保存1.25至2.75年,随后通过顶空气相色谱法进行分析。结果显示直接测定和延迟乙醇测定之间总体相关性良好(r = 0.900)。警官按照既定方案收集样本,给出结果以说明该技术的实际应用和局限性。

相似文献

1
A long-term field experience with breath ethanol collection employing silica gel.使用硅胶进行呼气乙醇收集的长期实地经验。
J Anal Toxicol. 1986 Sep-Oct;10(5):194-7. doi: 10.1093/jat/10.5.194.
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Delayed ethanol analysis of breath specimens: long-term field experience with commercial silica gel tubes and breathalyzer collection.
J Forensic Sci. 1990 Nov;35(6):1353-9.
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In vitro accuracy and precision studies comparing direct and delayed analysis of the ethanol content of vapor.比较蒸汽中乙醇含量直接分析和延迟分析的体外准确性和精密度研究。
J Forensic Sci. 1987 Jan;32(1):48-54.
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Observations on ToxTrap silica gel breath capture tubes for alcohol analysis.用于酒精分析的ToxTrap硅胶呼气捕获管的观察报告。
J Forensic Sci. 1985 Jan;30(1):186-93.
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Selection of a suitable internal standard in head space gas chromatographic breath ethanol analysis after adsorption on silica gel.硅胶吸附后顶空气相色谱法测定呼出气体乙醇时合适内标物的选择。
Blutalkohol. 1986 Mar;23(2):138-42.
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Breath alcohol analysis: interlaboratory evaluation of silica gel as trapping system.呼气酒精分析:硅胶作为捕集系统的实验室间评估
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Alcohol analysis of stored whole-breath samples by automated gas chromatography.通过自动气相色谱法对储存的全呼吸样本进行酒精分析。
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