以吸附在硅胶上的白蛋白作为固定相，对映体的直接分析和制备拆分。
Direct analytical and preparative resolution of enantiomers using albumin adsorbed to silica as a stationary phase.
作者信息
Erlandsson P, Hansson L, Isaksson R
出版信息
J Chromatogr. 1986 Dec 24;370(3):475-83. doi: 10.1016/s0021-9673(00)94717-4.
PMID:3029151
Abstract
A rapid and simple method for the preparation of high-performance liquid chromatography columns for chiral separations is described. The stationary phase is prepared by adsorbing bovine serum albumin on silica. Both analytical and preparative applications are described. A polarimeter was used as a detector to determine the enantiomer elution orders.
摘要
本文描述了一种快速简便的制备用于手性分离的高效液相色谱柱的方法。固定相通过将牛血清白蛋白吸附在硅胶上制备而成。文中介绍了该方法在分析和制备方面的应用。使用旋光仪作为检测器来确定对映体的洗脱顺序。
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