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纳米金刚石添加对 PMMA 义齿基托的挠曲强度、冲击强度和表面粗糙度的影响。

Effect of Nanodiamond Addition on Flexural Strength, Impact Strength, and Surface Roughness of PMMA Denture Base.

机构信息

Department of Substitutive Dental Sciences, College of Dentistry, Imam Abdulrahman Bin Faisal University, Dammam, Saudi Arabia.

Advanced Education Program in Prosthodontics, Loma Linda University School of Dentistry, Loma Linda, CA.

出版信息

J Prosthodont. 2019 Jan;28(1):e417-e425. doi: 10.1111/jopr.12969. Epub 2018 Oct 23.

Abstract

PURPOSE

To assess the effect of addition of different concentrations of nanodiamonds (NDs) on flexural strength, impact strength, and surface roughness of heat-polymerized acrylic resin.

MATERIALS AND METHODS

120 specimens were fabricated from heat-polymerized acrylic resin. They were divided into a control group of pure polymethylmethacrylate (PMMA; Major.Base.20) and three tested groups (PMMA-ND) with 0.5%wt, 1%wt, and 1.5%wt of added ND to PMMA. Flexural strength was determined using the three-point bending test. Impact strength was recorded by using a Charpy type impact test. Surface roughness test was performed using a Contour GT machine. One-way ANOVA and Tukey's post-hoc analysis (p ≤ 0.05) were used for statistical analysis.

RESULTS

Acrylic resin reinforced with 0.5% ND displayed significantly higher flexural strength than the unreinforced heat-polymerized specimens, acrylic resin reinforced with 1% ND and the 1.5% ND (p < 0.0001). The impact strength of unreinforced heat-polymerized specimens was significantly higher than all nano-composite materials (p < 0.0001) with no significant difference between 1% ND and the 1.5% ND (p > 0.05). The addition of 0.5% ND and 1% ND significantly decreased the surface roughness in comparison to both control and the 1.5% ND groups (p < 0.0001) while no significant differences between 0.5% ND and 1% ND (p > 0.05) were reported. Nano-composite material (0.5% ND) showed significantly lower surface roughness when compared to other specimens.

CONCLUSIONS

The addition of NDs to acrylic denture base improved the flexural strength and surface roughness at low concentrations (0.5%), while the impact strength was decreased with ND addition.

摘要

目的

评估不同浓度纳米金刚石(NDs)对热聚合丙烯酸树脂弯曲强度、冲击强度和表面粗糙度的影响。

材料与方法

用热聚合丙烯酸树脂制作 120 个试件,分为纯聚甲基丙烯酸甲酯(PMMA;Major.Base.20)对照组和 3 个实验组(PMMA-ND),每组分别添加 0.5%wt、1%wt 和 1.5%wt 的 ND 到 PMMA 中。用三点弯曲试验测定弯曲强度,用夏比冲击试验记录冲击强度,用轮廓 GT 机进行表面粗糙度试验。采用单因素方差分析和 Tukey 事后检验(p≤0.05)进行统计学分析。

结果

添加 0.5%ND 的丙烯酸树脂的弯曲强度明显高于未增强的热聚合试件、添加 1%ND 和 1.5%ND 的丙烯酸树脂(p<0.0001)。未增强的热聚合试件的冲击强度明显高于所有纳米复合材料(p<0.0001),而 1%ND 和 1.5%ND 之间无显著差异(p>0.05)。与对照组和 1.5%ND 组相比,添加 0.5%ND 和 1%ND 可显著降低表面粗糙度(p<0.0001),但 0.5%ND 和 1%ND 之间无显著差异(p>0.05)。纳米复合材料(0.5%ND)的表面粗糙度明显低于其他试件。

结论

在低浓度(0.5%)下,NDs 的添加提高了丙烯酸义齿基托的弯曲强度和表面粗糙度,而 ND 的添加降低了冲击强度。

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