Department of Substitutive Dental Sciences, College of Dentistry, Imam Abdulrahman Bin Faisal University, Dammam, Saudi Arabia.
Advanced Education Program in Prosthodontics, Loma Linda University School of Dentistry, Loma Linda, CA.
J Prosthodont. 2019 Jan;28(1):e417-e425. doi: 10.1111/jopr.12969. Epub 2018 Oct 23.
To assess the effect of addition of different concentrations of nanodiamonds (NDs) on flexural strength, impact strength, and surface roughness of heat-polymerized acrylic resin.
120 specimens were fabricated from heat-polymerized acrylic resin. They were divided into a control group of pure polymethylmethacrylate (PMMA; Major.Base.20) and three tested groups (PMMA-ND) with 0.5%wt, 1%wt, and 1.5%wt of added ND to PMMA. Flexural strength was determined using the three-point bending test. Impact strength was recorded by using a Charpy type impact test. Surface roughness test was performed using a Contour GT machine. One-way ANOVA and Tukey's post-hoc analysis (p ≤ 0.05) were used for statistical analysis.
Acrylic resin reinforced with 0.5% ND displayed significantly higher flexural strength than the unreinforced heat-polymerized specimens, acrylic resin reinforced with 1% ND and the 1.5% ND (p < 0.0001). The impact strength of unreinforced heat-polymerized specimens was significantly higher than all nano-composite materials (p < 0.0001) with no significant difference between 1% ND and the 1.5% ND (p > 0.05). The addition of 0.5% ND and 1% ND significantly decreased the surface roughness in comparison to both control and the 1.5% ND groups (p < 0.0001) while no significant differences between 0.5% ND and 1% ND (p > 0.05) were reported. Nano-composite material (0.5% ND) showed significantly lower surface roughness when compared to other specimens.
The addition of NDs to acrylic denture base improved the flexural strength and surface roughness at low concentrations (0.5%), while the impact strength was decreased with ND addition.
评估不同浓度纳米金刚石(NDs)对热聚合丙烯酸树脂弯曲强度、冲击强度和表面粗糙度的影响。
用热聚合丙烯酸树脂制作 120 个试件,分为纯聚甲基丙烯酸甲酯(PMMA;Major.Base.20)对照组和 3 个实验组(PMMA-ND),每组分别添加 0.5%wt、1%wt 和 1.5%wt 的 ND 到 PMMA 中。用三点弯曲试验测定弯曲强度,用夏比冲击试验记录冲击强度,用轮廓 GT 机进行表面粗糙度试验。采用单因素方差分析和 Tukey 事后检验(p≤0.05)进行统计学分析。
添加 0.5%ND 的丙烯酸树脂的弯曲强度明显高于未增强的热聚合试件、添加 1%ND 和 1.5%ND 的丙烯酸树脂(p<0.0001)。未增强的热聚合试件的冲击强度明显高于所有纳米复合材料(p<0.0001),而 1%ND 和 1.5%ND 之间无显著差异(p>0.05)。与对照组和 1.5%ND 组相比,添加 0.5%ND 和 1%ND 可显著降低表面粗糙度(p<0.0001),但 0.5%ND 和 1%ND 之间无显著差异(p>0.05)。纳米复合材料(0.5%ND)的表面粗糙度明显低于其他试件。
在低浓度(0.5%)下,NDs 的添加提高了丙烯酸义齿基托的弯曲强度和表面粗糙度,而 ND 的添加降低了冲击强度。