Bharti D B, Bharati Avinash V, Wankhade Atul V
J D College of Engineering and Management and Shree ramdeobaba College of Engineering and Management, Nagpur, India.
Shree Ramdeobaba College of Engineering and Management, Nagpur, India.
Luminescence. 2018 Dec;33(8):1445-1449. doi: 10.1002/bio.3572. Epub 2018 Oct 30.
Microwave-assisted routes have attracted much attention for nanoparticle synthesis because of minimal solvent use and rapid, high efficiency and controlled morphology. Cadmium sulphide (CdS) nanoparticles form the line between bulk and molecular states of materials and show variation in their physical and chemical properties. Cadmium sulphate and thiourea were used as precursors during this synthesis. These are included in the category of practical semiconductor metal sulphides, which are extensively used as catalysts and optical materials. X-ray diffraction (XRD) patterns confirmed that CdO nanoparticles are crystalline and have a hexagonal phase with crystal sizes that agree with transmission electron microscopy (TEM) data. UV-visible spectroscopy and photoluminescence (PL) spectroscopy were used to evaluate optical properties using band gap energy measurements.
微波辅助路线因溶剂使用量少、快速、高效且能控制形态,在纳米颗粒合成中备受关注。硫化镉(CdS)纳米颗粒处于材料的体相和分子态之间,其物理和化学性质存在差异。在此合成过程中,硫酸镉和硫脲被用作前驱体。它们属于实用的半导体金属硫化物类别,被广泛用作催化剂和光学材料。X射线衍射(XRD)图谱证实,CdO纳米颗粒是晶体,具有六方相,其晶体尺寸与透射电子显微镜(TEM)数据相符。紫外可见光谱和光致发光(PL)光谱用于通过带隙能量测量来评估光学性质。