Laboratory of Bioorganic Chemistry, Department of Physics, Università degli Studi di Trento, Trento, Italy.
Institute of Chemistry, Academy of Sciences of Moldova, Chisinau, Republic of Moldova.
Nat Prod Res. 2020 Jan;34(2):290-295. doi: 10.1080/14786419.2018.1530227. Epub 2018 Nov 17.
The phenylethanoids rostkovianoside, 6'--acetylcrassifolioside and the flavonoid rutin 3‴-acetate, were isolated from the methanolic extract of the aerial parts of Hayne. The structures of these previously undescribed compounds were elucidated by interpretation of spectroscopic data. The acetylation of rutin was also carried out and four ester derivatives were spectroscopically characterized. Finally, a chromatographic method was established to easily identify the acetylated position.
从 Hayne 地上部分的甲醇提取物中分离得到苯乙醇苷 rostkovianoside、6'--乙酰 crassifolioside 和黄酮芦丁 3‴-乙酸酯。通过对光谱数据的解释,阐明了这些以前未描述的化合物的结构。芦丁也进行了乙酰化,并用光谱法对四个酯衍生物进行了表征。最后,建立了一种色谱方法,可轻松鉴定乙酰化位置。