Balashov T, Meyer M, Wulfhekel W
Physikalisches Institut, Karlsruhe Institute of Technology, Wolfgang-Gaede-Strasse 1, 76131 Karlsruhe, Germany.
Rev Sci Instrum. 2018 Nov;89(11):113707. doi: 10.1063/1.5043636.
We have designed and built a scanning tunneling microscope (STM) setup for operation at millikelvin temperatures in an ultrahigh vacuum. A compact cryostat with an integrated dilution refrigerator has been built that allows measurements at a base temperature of 25 mK in the magnetic field up to 7.5 T with low mechanical and electronic noise. The cryostat is not larger than conventional helium bath cryostats (23 and 13 l of nitrogen and helium, respectively) so that the setup does not require a large experimental hall and fits easily into a standard lab space. Mechanical vibrations with running dilution circulation were kept below 1 pm/ by mechanically decoupling the STM from the cryostat and the pumping system. All electronic input lines were low-pass filtered, reducing the electronic temperature to below 100 mK, as deduced from the quasiparticle peaks of superconducting aluminum. The microscope is optically accessible in the parked position, making sample and tip exchange fast and user-friendly. For measurement, the STM is lowered 60 mm down so that the sample ends in the middle of a wet superconducting magnetic coil.
我们设计并搭建了一套扫描隧道显微镜(STM)装置,用于在超高真空中的毫开尔文温度下运行。已构建了一个带有集成稀释制冷机的紧凑型低温恒温器,它能够在高达7.5 T的磁场中,于25 mK的基础温度下进行测量,且机械和电子噪声较低。该低温恒温器不大于传统的氦浴低温恒温器(分别为23升氮气和13升氦气),因此该装置不需要大型实验厅,可轻松安装在标准实验室空间内。通过将STM与低温恒温器和泵系统进行机械解耦,使运行稀释循环时的机械振动保持在1 pm/ 以下。所有电子输入线路都进行了低通滤波,根据超导铝的准粒子峰推断,将电子温度降低至100 mK以下。显微镜在停放位置时可进行光学操作,使得样品和探针的更换快速且方便用户使用。进行测量时,将STM向下降低60 mm,以便样品位于湿式超导磁线圈的中间位置。