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一台在超高真空环境下配备绝热去磁制冷的毫开尔文扫描隧道显微镜。

A millikelvin scanning tunneling microscope in ultra-high vacuum with adiabatic demagnetization refrigeration.

作者信息

Esat Taner, Borgens Peter, Yang Xiaosheng, Coenen Peter, Cherepanov Vasily, Raccanelli Andrea, Tautz F Stefan, Temirov Ruslan

机构信息

Peter Grünberg Institute (PGI-3), Forschungszentrum Jülich, 52425 Jülich, Germany.

Cryovac GmbH & Co KG, 53842 Troisdorf, Germany.

出版信息

Rev Sci Instrum. 2021 Jun 1;92(6):063701. doi: 10.1063/5.0050532.

DOI:10.1063/5.0050532
PMID:34243501
Abstract

We present the design and performance of an ultra-high vacuum scanning tunneling microscope (STM) that uses adiabatic demagnetization of electron magnetic moments for controlling its operating temperature ranging between 30 mK and 1 K with an accuracy of up to 7 μK rms. At the same time, high magnetic fields of up to 8 T can be applied perpendicular to the sample surface. The time available for STM experiments at 50 mK is longer than 20 h, at 100 mK about 40 h. The single-shot adiabatic demagnetization refrigerator can be regenerated automatically within 7 h while keeping the STM temperature below 5 K. The whole setup is located in a vibrationally isolated, electromagnetically shielded laboratory with no mechanical pumping lines penetrating its isolation walls. The 1 K pot of the adiabatic demagnetization refrigeration cryostat can be operated silently for more than 20 days in a single-shot mode using a custom-built high-capacity cryopump. A high degree of vibrational decoupling together with the use of a specially designed minimalistic STM head provides outstanding mechanical stability, demonstrated by the tunneling current noise, STM imaging, and scanning tunneling spectroscopy measurements, all performed on an atomically clean Al(100) surface.

摘要

我们展示了一种超高真空扫描隧道显微镜(STM)的设计与性能,该显微镜利用电子磁矩的绝热去磁来控制其工作温度,温度范围在30 mK至1 K之间,均方根误差精度高达7 μK。同时,可在垂直于样品表面的方向施加高达8 T的强磁场。在50 mK下进行STM实验的可用时间超过20小时,在100 mK下约为40小时。单次绝热去磁制冷机可在7小时内自动再生,同时将STM温度保持在5 K以下。整个装置位于一个振动隔离、电磁屏蔽的实验室中,没有机械抽气管道穿透其隔离壁。绝热去磁制冷低温恒温器的1 K冷屏可使用定制的高容量低温泵以单次模式安静运行超过20天。高度的振动解耦以及使用特别设计的简约STM探头提供了出色的机械稳定性,这通过在原子级清洁的Al(100)表面上进行的隧道电流噪声、STM成像和扫描隧道谱测量得到了证明。

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