Geng Tao, Wang Jihao, Meng Wenjie, Zhang Jing, Feng Qiyuan, Hou Yubin, Lu Qingyou
High Magnetic Field Laboratory, Hefei Institutes of Physical Science, Chinese Academy of Sciences, Hefei 230031, China.
University of Science and Technology of China, Hefei 230026, China.
Micromachines (Basel). 2023 Mar 11;14(3):637. doi: 10.3390/mi14030637.
We present a novel homebuilt scanning tunneling microscope (STM) with atomic resolution integrated into a cryogen-free superconducting magnet system with a variable temperature insert. The STM head is designed as a nested structure of double piezoelectric tubes (PTs), which are connected coaxially through a sapphire frame whose top has a sample stage. A single shaft made of tantalum, with the STM tip on top, is held firmly by a spring strip inside the internal PT. The external PT drives the shaft to the tip-sample junction based on the SpiderDrive principle, and the internal PT completes the subsequent scanning and imaging work. The STM head is simple, compact, and easy to assemble. The excellent performance of the device was demonstrated by obtaining atomic-resolution images of graphite and low drift rates of 30.2 pm/min and 41.4 pm/min in the X-Y plane and Z direction, respectively, at 300K. In addition, we cooled the sample to 1.6 K and took atomic-resolution images of graphite and NbSe. Finally, we performed a magnetic field sweep test from 0 T to 9 T at 70 K, obtaining distinct graphite images with atomic resolution under varying magnetic fields. These experiments show our newly developed STM's high stability, vibration resistance, and immunity to high magnetic fields.
我们展示了一种新型的自制扫描隧道显微镜(STM),它具有原子分辨率,并集成到一个带有可变温度插入件的无液氦超导磁体系统中。STM探头设计为双压电管(PT)的嵌套结构,它们通过一个顶部带有样品台的蓝宝石框架同轴连接。一根由钽制成的单轴,顶部装有STM探针,由内部PT内的弹簧条牢固固定。外部PT基于SpiderDrive原理将轴驱动到探针 - 样品结处,内部PT完成后续的扫描和成像工作。STM探头结构简单、紧凑且易于组装。在300K时,通过获得石墨的原子分辨率图像以及在X - Y平面和Z方向上分别为30.2 pm/min和41.4 pm/min的低漂移率,证明了该设备的优异性能。此外,我们将样品冷却至1.6K,并拍摄了石墨和NbSe的原子分辨率图像。最后,我们在70K下进行了从0T到9T的磁场扫描测试,在不同磁场下获得了具有原子分辨率的清晰石墨图像。这些实验表明我们新开发的STM具有高稳定性、抗振性和对高磁场的免疫力。