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锂和磷对提高二硅酸锂和氧化锆之间粘结强度的衬垫效果的影响。

Effects of Lithium and Phosphorus on the Efficacy of a Liner for Increasing the Shear Bond Strength Between Lithium Disilicate and Zirconia.

出版信息

J Adhes Dent. 2018;20(6):535-540. doi: 10.3290/j.jad.a41629.

Abstract

PURPOSE

To evaluate the effect of the chemical formulation of liners on the shear bond strength (SBS) between lithium disilicate veneering ceramic and zirconia core.

MATERIALS AND METHODS

Four experimental groups (n = 12) were designed according to liner composition: negative control group (lithium and phosphorus removed from the conventional liner), Li group (lithium added to the negative control group), P group (phosphorus added to the negative control group), and Li+P group as the positive control (conventional liner). After applying the liner, lithium disilicate was pressed on zirconia. Specimens were stored in distilled water (37°C, 24 h) before testing the SBS. To test the SBS, shear force was applied perpendicular to the lithium disilicate-zirconia interface. The differences in the SBS between the veneer lithium disilicate and zirconia substructure were evaluated with one-way ANOVA (significance level of 0.05).

RESULTS

The presence or absence of lithium and phosphorus influenced the efficacy of the liner. The negative control and P groups showed mainly cohesive failures, and the Li group mainly showed mixed failures. Both adhesive and mixed failures were observed in the Li+P group. The groups including lithium showed significantly higher SBS than the negative control or Li+P group (p < 0.05). The group including phosphorus, which showed higher crystallinity, showed significantly lower SBS than the negative control and Li+P groups (p < 0.05).

CONCLUSIONS

The differences in the composition of the liner can affect the wettability and reactivity, and as a result, the SBS was different.

摘要

目的

评估衬垫化学配方对二硅酸锂饰瓷与氧化锆基底间剪切结合强度(SBS)的影响。

材料与方法

根据衬垫成分设计了四个实验组(n=12):阴性对照组(从常规衬垫中去除锂和磷)、Li 组(在阴性对照组中添加锂)、P 组(在阴性对照组中添加磷)和 Li+P 组作为阳性对照(常规衬垫)。在施加衬垫后,将二硅酸锂压在氧化锆上。将样品储存在蒸馏水中(37°C,24 h),然后进行 SBS 测试。为了测试 SBS,沿二硅酸锂-氧化锆界面垂直施加剪切力。采用单因素方差分析(显著性水平 0.05)评估饰层二硅酸锂与氧化锆基层之间 SBS 的差异。

结果

锂和磷的存在或缺失影响了衬垫的效果。阴性对照组和 P 组主要表现为内聚性破坏,Li 组主要表现为混合性破坏。Li+P 组中观察到粘结性和混合性破坏。含有锂的组的 SBS 明显高于阴性对照组或 Li+P 组(p<0.05)。磷含量较高的组表现出明显较低的 SBS,低于阴性对照组和 Li+P 组(p<0.05)。

结论

衬垫成分的差异会影响润湿性和反应性,从而导致 SBS 不同。

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