Department of Food Engineering, Faculty of Engineering at Kamphaengsaen, Kasetsart University, Kamphaengsaen Campus, Nakhonpathom 73140, Thailand; School of Culinary Arts, Suan Dusit University, Bangkok 10700, Thailand.
Department of Food Engineering, Faculty of Engineering at Kamphaengsaen, Kasetsart University, Kamphaengsaen Campus, Nakhonpathom 73140, Thailand; Center of Advanced Studies in Industrial Technology, Kasetsart University, Bangkok 10900, Thailand.
Food Chem. 2019 Apr 25;278:364-372. doi: 10.1016/j.foodchem.2018.11.067. Epub 2018 Nov 13.
Microwave and conventional heating methods were used to extract pectin from lime peel waste using different acid extractants (hydrochloric or citric acid) and peel-to-extractant ratios (1:20 or 1:40). Hydrochloric acid as the extractant resulted in a higher yield of pectin with both methods. The methoxyl content and galacturonic acid content of lime peel pectin were in the range 8.74-10.51% and 79.29-95.93%, respectively. The intense band around 1730 cm corresponded to methyl esterified uronic carboxyl groups and confirmed the higher equivalent weight and degree of esterification for the microwave-extracted pectin than that from conventional extraction. Lime peel pectin could be classified as high methoxyl pectin having a rapid-set gel formation. The viscosity and viscoelastic properties of the pectin solution from both heating methods enhanced with increasing solid concentration. Hence, microwave heating can be a short processing time for pectin extraction from lime peel waste with suitable pectin properties.
采用微波和常规加热方法,使用不同的酸提取剂(盐酸或柠檬酸)和果皮与提取剂的比例(1:20 或 1:40),从橙皮废物中提取果胶。盐酸作为提取剂,两种方法都能得到更高产率的果胶。橙皮果胶的甲氧基含量和半乳糖醛酸含量分别在 8.74-10.51%和 79.29-95.93%范围内。1730 cm 左右的强带对应于甲酯化的糖醛酸羧基基团,证实了微波提取果胶的等效重和酯化度高于常规提取的果胶。橙皮果胶可归类为高甲氧基果胶,具有快速凝胶形成的特性。随着固形物浓度的增加,两种加热方法得到的果胶溶液的粘度和粘弹性都得到了增强。因此,微波加热可以在较短的加工时间内从橙皮废物中提取出具有合适果胶性能的果胶。