France N C, Holland P T, McGhie T K, Wallace M R
Department of Pathology, Waikato Hospital, Hamilton, New Zealand.
J Chromatogr. 1988 Dec 9;433:1-7. doi: 10.1016/s0378-4347(00)80579-4.
A capillary gas chromatographic method for plasma oxalate and an isotope dilution mass spectrometric reference method, both using the same tert.-butyldimethylsilyl derivatives, are described. Similar reference ranges for both were found (4.93 +/- 1.48 and 4.70 +/- 1.44 mumol/l, respectively), together with a close correlation for results covering a wide range of oxalate concentrations.
本文描述了一种用于测定血浆草酸盐的毛细管气相色谱法以及一种同位素稀释质谱参考方法，二者均使用相同的叔丁基二甲基甲硅烷基衍生物。发现二者具有相似的参考范围（分别为4.93±1.48和4.70±1.44μmol/L），并且在涵盖广泛草酸盐浓度的结果之间具有密切相关性。
