• 文献检索
  • 文档翻译
  • 深度研究
  • 学术资讯
  • Suppr Zotero 插件Zotero 插件
  • 邀请有礼
  • 套餐&价格
  • 历史记录
应用&插件
Suppr Zotero 插件Zotero 插件浏览器插件Mac 客户端Windows 客户端微信小程序
定价
高级版会员购买积分包购买API积分包
服务
文献检索文档翻译深度研究API 文档MCP 服务
关于我们
关于 Suppr公司介绍联系我们用户协议隐私条款
关注我们

Suppr 超能文献

核心技术专利:CN118964589B侵权必究
粤ICP备2023148730 号-1Suppr @ 2026

文献检索

告别复杂PubMed语法,用中文像聊天一样搜索,搜遍4000万医学文献。AI智能推荐,让科研检索更轻松。

立即免费搜索

文件翻译

保留排版,准确专业,支持PDF/Word/PPT等文件格式,支持 12+语言互译。

免费翻译文档

深度研究

AI帮你快速写综述,25分钟生成高质量综述,智能提取关键信息,辅助科研写作。

立即免费体验

Capillary gas chromatographic analysis of volatile and non-volatile organic acids from biological samples as the t-butyldimethylsilyl derivatives.

作者信息

Schooley D L, Kubiak F M, Evans J V

出版信息

J Chromatogr Sci. 1985 Sep;23(9):385-90. doi: 10.1093/chromsci/23.9.385.

DOI:10.1093/chromsci/23.9.385
PMID:4044765
Abstract

A quantitative procedure for the analysis of volatile organic acids and lactic acid in silage is described. The samples were extracted with diethyl ether, derivatized by t-butyldimethylsilylation, and then separated by capillary gas chromatography. The same procedure was useful for the identification by gas chromatography/mass spectrometry of organic acids in samples such as the metabolic fermentation products of anaerobic bacteria.

摘要

相似文献

1
Capillary gas chromatographic analysis of volatile and non-volatile organic acids from biological samples as the t-butyldimethylsilyl derivatives.
J Chromatogr Sci. 1985 Sep;23(9):385-90. doi: 10.1093/chromsci/23.9.385.
2
Gas-liquid chromatography and mass spectral analysis of mono-, di- and tricarboxylates as their tert.-butyldimethylsilyl derivatives.作为叔丁基二甲基硅烷基衍生物的单羧酸盐、二羧酸盐和三羧酸盐的气-液色谱和质谱分析。
J Chromatogr. 1986 Jun 27;361:117-30. doi: 10.1016/s0021-9673(01)86899-0.
3
Analysis of amino acids by gas-liquid chromatography as tert.-butyldimethylsilyl derivatives. Preparation of derivatives in a single reaction.
J Chromatogr. 1987 Jan 30;387:241-53. doi: 10.1016/s0021-9673(01)94528-5.
4
Use of t-butyldimethylsilylation in the gas chromatographic/mass spectrometric analysis of physiologic compounds found in plasma using electron-impact ionization.
Anal Biochem. 1984 Aug 15;141(1):101-9. doi: 10.1016/0003-2697(84)90431-7.
5
Capillary gas chromatography of amino acids, including asparagine and glutamine: sensitive gas chromatographic-mass spectrometric and selected ion monitoring gas chromatographic-mass spectrometric detection of the N,O(S)-tert.-butyldimethylsilyl derivatives.氨基酸的毛细管气相色谱法,包括天冬酰胺和谷氨酰胺:N,O(S)-叔丁基二甲基甲硅烷基衍生物的灵敏气相色谱-质谱联用和选择离子监测气相色谱-质谱联用检测
J Chromatogr. 1987 Apr 17;392:249-58. doi: 10.1016/s0021-9673(01)94270-0.
6
Determination on the microscale of plasmatic lactic acid as its t-butyldimethylsilyl derivative by stable-isotope dilution using capillary gas chromatography/mass spectrometry.
Rapid Commun Mass Spectrom. 1992 Dec;6(12):781-3. doi: 10.1002/rcm.1290061214.
7
Simultaneous analysis of amino and organic acids in extracts of plant leaves as tert-butyldimethylsilyl derivatives by capillary gas chromatography.通过毛细管气相色谱法同时分析植物叶片提取物中作为叔丁基二甲基甲硅烷基衍生物的氨基酸和有机酸。
Anal Biochem. 1998 Jun 1;259(2):203-11. doi: 10.1006/abio.1998.2659.
8
Measurement of plasma oxalate by capillary gas chromatography and its validation by isotope dilution mass spectrometry.采用毛细管气相色谱法测定血浆草酸盐并通过同位素稀释质谱法进行验证。
J Chromatogr. 1988 Dec 9;433:1-7. doi: 10.1016/s0378-4347(00)80579-4.
9
Mass spectrometry and chromatography of t-butyldimethylsilyl derivatives of cytokinin bases.细胞分裂素碱基的叔丁基二甲基硅烷基衍生物的质谱分析和色谱分析
Anal Biochem. 1986 Feb 15;153(1):85-96. doi: 10.1016/0003-2697(86)90065-5.
10
Use of tert.-butyldimethylsilyl derivatives for gas chromatographic-mass spectrometric analysis of dipeptides.叔丁基二甲基甲硅烷基衍生物在二肽气相色谱-质谱分析中的应用。
J Chromatogr. 1987 Aug 7;419:263-70. doi: 10.1016/0378-4347(87)80284-0.

引用本文的文献

1
Aldehydic contact poisons and alarm pheromone of the antCrematogaster scutellaris (Hymenoptera: Myrmicinae) : Enzyme-Mediated Production from acetate precursors.蚁 Crematogaster scutellaris 的醛类接触毒物和报警信息素(膜翅目:蚁科):从醋酸盐前体到酶介导的产物生成。
J Chem Ecol. 1989 May;15(5):1501-11. doi: 10.1007/BF01012379.
2
Analysis of volatile fatty acids in biological specimens by capillary column gas chromatography.
Lipids. 1987 Mar;22(3):195-200. doi: 10.1007/BF02537302.
3
Degradation of barley straw, ryegrass, and alfalfa cell walls by Clostridium longisporum and Ruminococcus albus.长孢梭菌和白色瘤胃球菌对大麦秸秆、黑麦草及苜蓿细胞壁的降解作用
Appl Environ Microbiol. 1989 Dec;55(12):3080-4. doi: 10.1128/aem.55.12.3080-3084.1989.
4
Compartmentation of acetyl CoA studied by analysis of tricarboxylic acid cycle acids and 3-hydroxybutyrate in bile of rats given [2,2,2-2H3]ethanol.通过分析给予[2,2,2-2H3]乙醇的大鼠胆汁中的三羧酸循环酸和3-羟基丁酸来研究乙酰辅酶A的区室化。
Biochem J. 1990 Jan 15;265(2):569-74. doi: 10.1042/bj2650569.