Wang Shunbo, Xu Hailong, Wang Yunyi, Kong Lingqi, Wang Zhaoxin, Liu Sihan, Zhang Jianhai, Zhao Hongwei
School of Mechanical and Aerospace Engineering, Jilin University, Changchun 130025, China.
Rev Sci Instrum. 2019 Jan;90(1):015117. doi: 10.1063/1.5054628.
A modularized cryogenic indentation apparatus was designed and created to study the deformation mechanisms and mechanical properties of materials at low temperatures. The indentation process is actuated by piezoelectric stack and flexure hinge, and the entire mechanical module is kept inside the vacuum chamber to prevent the occurrence of ice. Numerous issues including the effects of the application of cooling module and processes to diminish the temperature effect on the indentation tip were addressed. Several influential factors during temperature indentation were discussed. Tests on calibration specimen demonstrated the feasibility of the apparatus. Monocrystalline silicon and copper were tested using the current apparatus at temperatures ranging from room temperature to 150 K to show its main functions and usability.
设计并制造了一种模块化低温压痕装置,用于研究材料在低温下的变形机制和力学性能。压痕过程由压电堆栈和柔性铰链驱动,整个机械模块置于真空室内以防止结冰。解决了包括冷却模块应用的影响以及减少温度对压痕尖端影响的工艺等诸多问题。讨论了温度压痕过程中的几个影响因素。对标定试样的测试证明了该装置的可行性。使用当前装置在室温至150 K的温度范围内对单晶硅和铜进行了测试,以展示其主要功能和实用性。