Baek Min-Seok, Kim Hyung-Jun, Lee Kee-Ahn
Department of Materials Science and Engineering, Inha University, Incheon 22212, Republic of Korea.
Hybrid Material Processing Research Department, RIST, Pohang-si, Gyeongbuk 790-600, Republic of Korea.
J Nanosci Nanotechnol. 2019 Jul 1;19(7):3935-3942. doi: 10.1166/jnn.2019.16147.
This study is related to cold spray 3D printing (kinetic metallization) capable of manufacturing near-net shape material. Anisotropy on the compressive deformation behavior of pure copper materials manufactured using cold spray process was investigated. In addition, the deformed microstructures that change according to strain were analyzed with different direction (spraying direction, perpendicular direction). Cu bulk material manufactured through cold spray processes showed distinctive structures wherein high-density dislocations had been accumulated because individual powder particles collided at high speed. After compression with different direction, spraying direction showed 330 MPa yield strength, 437 MPa compressive peak stress and perpendicular direction showed 327 MPa (Y.S.), 422 MPa (C.P.S). In low strain condition, dynamic recovery occurred in internal dislocation structures, thereby showing strain softening phenomena even at room temperature. For a closed examine of anisotropy on the compressive deformation and fracture behavior, we used SEM, FE-SEM, XRD, EBSD and observed microstructure and fractography with different direction.
本研究涉及能够制造近净形材料的冷喷涂3D打印(动力金属化)。研究了采用冷喷涂工艺制造的纯铜材料压缩变形行为的各向异性。此外,还分析了不同方向(喷涂方向、垂直方向)上随应变变化的变形微观结构。通过冷喷涂工艺制造的铜块状材料呈现出独特的结构,其中由于单个粉末颗粒高速碰撞而积累了高密度位错。在不同方向压缩后,喷涂方向的屈服强度为330MPa,压缩峰值应力为437MPa,垂直方向的屈服强度为327MPa,压缩峰值应力为422MPa。在低应变条件下,内部位错结构发生动态回复,从而即使在室温下也呈现出应变软化现象。为了深入研究压缩变形和断裂行为的各向异性,我们使用了扫描电子显微镜(SEM)、场发射扫描电子显微镜(FE-SEM)、X射线衍射仪(XRD)、电子背散射衍射(EBSD),并观察了不同方向的微观结构和断口形貌。