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用球磨结合化学处理从可可椰子变种橘黄色果梗中提取纤维素纳米纤维。

Extraction of cellulose nanofibers from cocos nucifera var aurantiaca peduncle by ball milling combined with chemical treatment.

机构信息

Department of Mechanical Engineering, K.L.N. College of Engineering, Pottapalayam, Tamil Nadu, India.

Department of Mechanical Engineering, K.L.N. College of Engineering, Pottapalayam, Tamil Nadu, India.

出版信息

Carbohydr Polym. 2019 May 15;212:312-322. doi: 10.1016/j.carbpol.2019.02.063. Epub 2019 Feb 19.

Abstract

The development of bio-degradable, renewable and low-cost material is critical to meet the growing environmental concerns and energy demands. The present study emphasizes on the extraction of a new kind of Cellulose NanoFibers (CNFs) from peduncles which are a bio-waste product of Cocos nucifera var-Aurantiaca through ball milling combined with chemical treatment. The crystallinity index, presence of functional groups and elemental composition in CNFs were identified by employing XRD, FT-IR and EDX techniques. The thermal stability of CNFs was investigated by thermo-gravimetric analysis. The morphological analysis was performed by electron microscopy and the results showed the appearance of CNFs in web-like structure with a width of 55-64 nm. The effect of reinforcement of CNFs in epoxy matrix was performed, whose tensile strength increased by 37% when 2 wt% of CNFs was loaded into the matrix.

摘要

开发可生物降解、可再生和低成本的材料对于满足日益增长的环境问题和能源需求至关重要。本研究强调通过球磨结合化学处理从可可椰子变种-金心果的果柄中提取一种新型纤维素纳米纤维(CNFs),这是一种生物废料。通过 XRD、FT-IR 和 EDX 技术确定了 CNFs 的结晶度指数、官能团的存在和元素组成。通过热重分析研究了 CNFs 的热稳定性。通过电子显微镜进行了形态分析,结果表明 CNFs 呈网状结构,宽度为 55-64nm。研究了 CNFs 在环氧树脂基体中的增强效果,当基体中加入 2wt%的 CNFs 时,其拉伸强度提高了 37%。

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