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使用元素粉末混合物对Al0.5CrMoNbTa0.5高熵合金进行选择性电子束熔化。

Selective electron beam melting of Al0.5CrMoNbTa0.5 high entropy alloys using elemental powder blend.

作者信息

Popov Vladimir V, Katz-Demyanetz Alexander, Koptyug Andrey, Bamberger Menachem

机构信息

Israel Institute of Metals, Technion R&D Foundation, Technion City, 3200003, Haifa, Israel.

Sports Tech Research Centre, Mid Sweden University, Akademigatan1, SE-831 25, Östersund, Sweden.

出版信息

Heliyon. 2019 Feb 6;5(2):e01188. doi: 10.1016/j.heliyon.2019.e01188. eCollection 2019 Feb.

Abstract

High Entropy Alloys (HEAs) is a novel promising class of multi-component materials which may demonstrate superior mechanical properties useful for high-temperature applications. Despite the high potential of HEAs, their production is complicated, using pre-alloyed powders in powder metallurgy route. This significantly complicates development and implementation of refractory BCC solid solution based HEAs. The present paper reports on experiments aiming at production of Al0.5CrMoNbTa0.5 multi-principle alloy using powder bed beam based additive manufacturing. Samples were manufactured using Selective Electron Beam Melting (SEBM) additive manufacturing technique from a blend of elemental powders aiming at achieving microstructure with high configurational entropy. Though it was not possible to achieve completely homogeneous microstructure, the as-printed material was composed of the zones with two multi-component solid solutions, which differed only by Al content confirming alloying. The process parameters optimization was not carried out and the as-print material contained a notable amount of residual porosity. It was possible to reach lower porosity level using heat treatment at 1300 °C for 24 hours, however undesirable alloy composition changes took place. The main conclusion is that the production of the Al0.5CrMoNbTa0.5 multi-principle alloy from elemental powder blends using SEBM technique is achievable, but the process parameter optimization rather than post-process heat treatment should be performed to reduce the porosity of samples.

摘要

高熵合金(HEAs)是一类新型且有前景的多组分材料,其可能展现出适用于高温应用的优异机械性能。尽管高熵合金具有很高的潜力,但其生产过程复杂,在粉末冶金路线中使用预合金粉末。这显著地使基于难熔体心立方固溶体的高熵合金的开发与应用变得复杂。本文报道了旨在使用基于粉末床束的增材制造来生产Al0.5CrMoNbTa0.5多主元合金的实验。样品是使用选择性电子束熔化(SEBM)增材制造技术,由元素粉末混合物制造而成,旨在获得具有高组态熵的微观结构。尽管不可能实现完全均匀的微观结构,但打印后的材料由具有两种多组分固溶体的区域组成,这两种固溶体仅在铝含量上有所不同,证实了合金化。未进行工艺参数优化,打印后的材料含有大量残余孔隙。在1300℃下进行24小时的热处理可以达到较低的孔隙率水平,然而发生了不理想的合金成分变化。主要结论是,使用SEBM技术从元素粉末混合物中生产Al O.5CrMoNbTa0.5多主元合金是可行的,但应进行工艺参数优化而非后处理热处理来降低样品的孔隙率。 (注:原文中“Al0.5CrMoNbTa0.5”中的“Al O.5”疑似有误,应为“Al0.5”,译文按正确理解翻译)

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c876/6366149/964f3943d2b9/gr1.jpg

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