Charasseangpaisarn Taksid, Wiwatwarrapan Chairat, Leklerssiriwong Nonthida
Department of Prosthodontics, Faculty of Dentistry, Chulalongkorn University, Bangkok, Thailand.
Department of Dentistry, Khon Kaen Hospital, Khon Kaen, Thailand.
J Dent Sci. 2016 Dec;11(4):443-448. doi: 10.1016/j.jds.2016.07.003. Epub 2016 Nov 14.
BACKGROUND/PURPOSE: The residual monomer remaining in acrylic resin can cause an allergic reaction and is toxic to oral soft tissue. This study determined the effect of the duration of ultrasonic cleaning on the amount of residual methyl methacrylate monomer in one heat-polymerized acrylic resin, Meliodent, and three autopolymerized acrylic resins, Unifast Trad Ivory, Unifast Trad Pink, and Unifast III.
Thirty-six disc-shaped specimens of each brand were prepared and randomly divided into six groups: control (no treatment), positive control, and ultrasonic treatment in 50°C water for 3 minutes, 5 minutes, 10 minutes, or 15 minutes. The residual monomer was extracted and analyzed using high performance liquid chromatography.
There were no significant differences in the residual monomer amount in the Meliodent groups. The amounts of residual monomer in the autopolymerized acrylic resin positive control group and ultrasonic treatment groups were significantly lower than those of the control group for the Unifast Trad Ivory, Unifast Trad Pink, and Unifast III groups (P < 0.05). The amount of residual monomer was not significantly different between the ultrasonic treatment in 50°C water (3 minutes for Unifast Trad Pink and 5 minutes for Unifast Trad Ivory and Unifast III) groups and the positive control group (P > 0.05).
Ultrasonic treatment with 50°C water for 3-5 minutes for autopolymerized resin and 3 minutes for heat-polymerized acrylic resin reduced the amount of residual monomer similarly to previously recommended methods, using shorter treatment times.
背景/目的:丙烯酸树脂中残留的单体可引起过敏反应,且对口腔软组织有毒性。本研究测定了超声清洗时长对一种热固化丙烯酸树脂(Meliodent)以及三种自固化丙烯酸树脂(Unifast Trad Ivory、Unifast Trad Pink和Unifast III)中甲基丙烯酸甲酯残留单体量的影响。
制备每个品牌的36个圆盘形试件,并随机分为六组:对照组(未处理)、阳性对照组,以及在50°C水中超声处理3分钟、5分钟、10分钟或15分钟的组。使用高效液相色谱法提取并分析残留单体。
Meliodent组的残留单体量无显著差异。对于Unifast Trad Ivory、Unifast Trad Pink和Unifast III组,自固化丙烯酸树脂阳性对照组和超声处理组的残留单体量显著低于对照组(P < 0.05)。在50°C水中超声处理组(Unifast Trad Pink为3分钟,Unifast Trad Ivory和Unifast III为5分钟)与阳性对照组之间的残留单体量无显著差异(P > 0.05)。
对于自固化树脂,在50°C水中超声处理3 - 5分钟,对于热固化丙烯酸树脂超声处理3分钟,与先前推荐的方法相比,能以更短的处理时间类似地减少残留单体量。