Du Zhaoxin, Ma Yan, Liu Fei, Xu Ning, Chen Yanfei, Wang Xiaopeng, Chen Yuyong, Gong Tianhao, Xu Dong
School of Materials Science and Engineering, Inner Mongolia University of Technology, Hohhot 010051, China.
Lab of Light-Weight Novel Materials, Inner Mongolia Metallic Materials Research Institute; Ningbo 315100, China.
Materials (Basel). 2019 May 7;12(9):1478. doi: 10.3390/ma12091478.
The influences of process annealing temperature during cold rolling on microstructure and mechanical properties of Ti-3.5Al-5Mo-6V-3Cr-2Sn-0.5Fe near β high strength titanium alloy sheets have been investigated. Results showed that the alloy mainly included the deformation induced dislocation structures after cold rolling but no obvious band structure, twin crystal or martensite were observed in this work. The texture components, which were affected by process annealing, are mainly γ-fiber, α-fiber and weak Goss texture. The γ-fiber of alloy when process annealed at 780 °C (α/β phase field) is stronger than at 830 °C (β phase field), where the Goss texture of alloy with process annealing temperature of 830 °C is more obvious. Results of annealing heat treatments showed that the recrystallization of the cold rolled was basically completed in a relatively short time of 2 min at 750 °C for 2 min. The refinement of grain size led to a significant increase of plasticity compared to rolled alloy. Results of tensile testing of aged alloy display the excellent combination of strength and plasticity, and the cold rolled alloy with process annealed at α/β phase field exhibits the better mechanical properties than at β phase field.
研究了冷轧过程中的工艺退火温度对Ti-3.5Al-5Mo-6V-3Cr-2Sn-0.5Fe近β型高强度钛合金板材微观组织和力学性能的影响。结果表明,冷轧后合金主要包含形变诱导位错组织,未观察到明显的带状组织、孪晶或马氏体。受工艺退火影响的织构组分主要为γ纤维、α纤维和较弱的高斯织构。合金在780℃(α/β相区)进行工艺退火时的γ纤维比在830℃(β相区)时更强,其中工艺退火温度为830℃的合金的高斯织构更明显。退火热处理结果表明,在750℃保温2 min的较短时间内,冷轧的再结晶基本完成。与轧制态合金相比,晶粒细化导致塑性显著提高。时效合金的拉伸试验结果显示出强度和塑性的优异结合,在α/β相区进行工艺退火的冷轧合金比在β相区具有更好的力学性能。