Meng Wenjie, Wang Jihao, Hou Yubin, Sui Mengqiao, Zhou Haibiao, Wang Junting, Wu Gang, Zhang Jing, Chen Fangchu, Luo Xuan, Sun Yupin, Li Junyun, Lu Qingyou
Anhui Province Key Laboratory of Condensed Matter Physics at Extreme Conditions, High Magnetic Field Laboratory of the Chinese Academy of Sciences, Hefei, Anhui 230031, People's Republic of China; CASmF Sci.&Tech. Ltd. (), Hefei, Anhui 230088, People's Republic of China.
Anhui Province Key Laboratory of Condensed Matter Physics at Extreme Conditions, High Magnetic Field Laboratory of the Chinese Academy of Sciences, Hefei, Anhui 230031, People's Republic of China; CASmF Sci.&Tech. Ltd. (), Hefei, Anhui 230088, People's Republic of China.
Ultramicroscopy. 2019 Oct;205:20-26. doi: 10.1016/j.ultramic.2019.06.006. Epub 2019 Jun 11.
We present a probe-type scanning tunnelling microscope (STM) with atomic resolution that is designed to be directly inserted and work in a harsh vibrational cryogen-free superconducting magnet system. When a commercial variable temperature insert (VTI) is installed in the magnet and the STM is housed in the VTI, a lowest temperature of 1.6 K can be achieved, at which the STM still operates well. We tested the STM in an 8 T superconducting magnet cooled with a pulse-tube cryocooler and obtained atomically resolved graphite and NbSe images as well as the scanning tunnelling spectrum (i.e., dI/dV spectrum) data of the latter near its critical temperature, which show the formation process of the superconducting gap as a function of temperature. The drifting rates of the STM at 1.6 K in the X-Y plane and Z direction are 1.15 and 1.71 pm/min, respectively. Noise analysis for the tunnelling current shows that the amplitudes of the dominant peaks (6.84 and 10.25 Hz) are as low as 1.5 pA.Hz when we set the current to 0.5 nA and open the feedback loop. This is important as a cryogen-free magnet system has long been considered too harsh for any atomic resolution measurement.
我们展示了一种具有原子分辨率的探针型扫描隧道显微镜(STM),其设计目的是直接插入并在恶劣振动的无液氦超导磁体系统中工作。当在磁体中安装商用变温插入件(VTI)并将STM置于VTI中时,可实现1.6 K的最低温度,在此温度下STM仍能良好运行。我们在由脉冲管制冷机冷却的8 T超导磁体中对STM进行了测试,获得了原子分辨的石墨和NbSe图像以及后者在其临界温度附近的扫描隧道谱(即dI/dV谱)数据,这些数据显示了超导能隙随温度的形成过程。STM在1.6 K时在X-Y平面和Z方向的漂移率分别为1.15和1.71 pm/min。对隧道电流的噪声分析表明,当我们将电流设置为0.5 nA并打开反馈回路时,主导峰(6.84和10.25 Hz)的幅度低至1.5 pA.Hz。这很重要,因为长期以来,无液氦磁体系统一直被认为对任何原子分辨率测量来说都过于恶劣。