Wei Lijun, Han Baoshuai, Ye Fan, Xu Yanjin, Wu Sujun
School of Material Science and Engineering, Beihang University, Beijing 100083, China.
Material Department, AVIC Manufacturing Technology Institute, Beijing 100024, China.
Materials (Basel). 2019 Jul 10;12(14):2229. doi: 10.3390/ma12142229.
The effect of high pressure (135 MPa) and the following heat treatment on the microstructure and micro-hardness of the squeezing cast AlSi9CuMg alloy is investigated, using optical microscopy (OM), Vickers tester, scanning electron microscopy (SEM), and transmission electron microscopy (TEM). The results indicate that the application of high pressure can increase under-cooling and the cooling rate during solidification and cause the refinement of the microstructure. The enhanced melt flow resulting from high pressure can also break the dendrite to form the spherical and elliptical primary α (Al) grains during the early stage of solidification. The winter-sweet flower-shaped primary α (Al) phases can also be formed through plastic deformation caused by the flow of the partially solidified melt. The ageing treatment results showed that a maximum (peak) micro-hardness value was obtained for each of the three ageing temperatures at different ageing times, and the highest peak value was achieved at 175 °C for 480 min. The micro-hardness change of the sample under different ageing processes was attributed to the variation of type, density, and size of the precipitates.
研究了高压(135MPa)及随后的热处理对挤压铸造AlSi9CuMg合金微观结构和显微硬度的影响,采用了光学显微镜(OM)、维氏硬度计、扫描电子显微镜(SEM)和透射电子显微镜(TEM)。结果表明,施加高压可增加凝固过程中的过冷度和冷却速率,并导致微观结构细化。高压导致的熔体流动增强还可在凝固早期使枝晶破碎,形成球形和椭圆形的初生α(Al)晶粒。部分凝固熔体的流动引起的塑性变形也可形成腊梅花样的初生α(Al)相。时效处理结果表明,在不同时效时间下,三种时效温度下的每一种都获得了最大(峰值)显微硬度值,在175℃时效480min时达到最高峰值。样品在不同时效过程中的显微硬度变化归因于析出相的类型、密度和尺寸的变化。