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[植物药中有机氯化合物残留量的分析。3. 通过填充柱和毛细管柱气相色谱法及气相色谱-质谱联用比较鉴定多氯联苯化合物残留量]

[Analysis of residues of organochlorine compounds in plant drugs. 3. Identification of residues of polychlorobiphenyl compounds by comparison of gas chromatography on packed and capillary columns and GCMS coupling].

作者信息

Benecke R, Brotka J, Wijsbeek J, Franke J P, Bruins A P, de Zeeuw R A

机构信息

Sektion Biowissenschaften der Karl-Marx-Universität Leipzig.

出版信息

Pharmazie. 1988 Feb;43(2):123-5.

PMID:3134665
Abstract

The identification of residues of polychlorinated biphenyls in a test sample of Flores Chamomillae could be achieved by the retention behavior at gas chromatographic analyses on packed and capillary columns compared with reference standard Clophen A 60, respectively as well as well by capillary GC/MS using single ion monitoring of substance-characteristic ion mass.

摘要

通过在填充柱和毛细管柱上进行气相色谱分析时与参考标准物质氯芬A 60的保留行为对比,以及通过毛细管气相色谱/质谱联用仪利用物质特征离子质量的单离子监测,可实现对洋甘菊测试样品中多氯联苯残留的鉴定。

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[Analysis of residues of organochlorine compounds in plant drugs. 3. Identification of residues of polychlorobiphenyl compounds by comparison of gas chromatography on packed and capillary columns and GCMS coupling].[植物药中有机氯化合物残留量的分析。3. 通过填充柱和毛细管柱气相色谱法及气相色谱-质谱联用比较鉴定多氯联苯化合物残留量]
Pharmazie. 1988 Feb;43(2):123-5.
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[Residues of organochlorine compounds in plant drugs. 1. Gas chromatographic determination of residues of organochlorine insecticides].
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[Blood PCB analysis by capillary column-gas chromatograph/quadruple mass spectrometer--comparison with packed column-electron capture detector/gas chromatograph].[采用毛细管柱-气相色谱仪/四极杆质谱仪分析血液中的多氯联苯——与填充柱-电子捕获检测器/气相色谱仪的比较]
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Application of gas chromatography-triple quadrupole mass spectrometry in the quantification-confirmation of pesticides and polychlorinated biphenyls in eggs at trace levels.气相色谱 - 三重四极杆质谱法在痕量水平鸡蛋中农药和多氯联苯定量确证中的应用
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Simultaneous analysis of polychlorinated biphenyls and organochlorine pesticides in water by headspace solid-phase microextraction with gas chromatography-tandem mass spectrometry.顶空固相微萃取-气相色谱-串联质谱法同时分析水中的多氯联苯和有机氯农药
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Enantiomeric separation of chiral polychlorinated biphenyls on beta-cyclodextrin capillary columns by means of heart-cut multidimensional gas chromatography and comprehensive two-dimensional gas chromatography. Application to food samples.通过中心切割多维气相色谱法和全二维气相色谱法在β-环糊精毛细管柱上对手性多氯联苯进行对映体分离。应用于食品样品。
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[Evaluation of the usefulness of SIS and MS/MS mode for the determination of persistent organochlorine compounds and polychlorinated biphenyls in human specimens].[评估单离子监测(SIS)和串联质谱(MS/MS)模式在测定人体样本中持久性有机氯化合物和多氯联苯方面的实用性]
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