Zhou Jianyu, Roberts O Steven, Goldwasser Samuel M, Lei Xia, Bokka Sreevalli, Chase George G
Department of Chemical and Biomolecular Engineering, The University of Akron, 185 E. Mill St., Akron, Ohio 44325-3906, USA.
Laser Teaching Center, Stony Brook University, 100 Nicolls Road, Stony Brook, New York 11794-0001, USA.
Rev Sci Instrum. 2019 Jul;90(7):075110. doi: 10.1063/1.5100137.
Thickness is an important characteristic parameter of electrospun submicron of fiber mats and membranes. The thickness of the mats directly influences performance properties such as permeability and is necessary when determining volumetric parameters such as porosity. Typical electrospun mats are very thin (less than 1 mm) and highly compressive due to the small diameter fibers, both of which make accurate measurements difficult when using conventional methods. An accurate measure of the thickness is desired for characterizing and comparing membrane performances. In this work, a thickness measurement instrument using laser interferometry has been designed to measure electrospun fiber mat thickness. A small disk is used to apply a small (reproducible) force applied across a reasonably small area of the fiber mat. A traversing pin moves to contact the disk and completes an electrical circuit to stop movement and determine the location of the disk relative to a reference plane. The fiber mat thickness is determined by measuring the difference in locations of the disk with and without the fiber mat between the disk and the reference plane. The prototype is simple to operate and user-friendly. Precision and accuracy of the prototype are discussed.
厚度是电纺亚微米纤维毡和膜的一个重要特征参数。毡的厚度直接影响诸如渗透性等性能,并且在确定诸如孔隙率等体积参数时是必要的。典型的电纺毡非常薄(小于1毫米),并且由于纤维直径小而具有高度压缩性,这两者使得使用传统方法进行精确测量变得困难。为了表征和比较膜的性能,需要精确测量厚度。在这项工作中,设计了一种使用激光干涉测量法的厚度测量仪器来测量电纺纤维毡的厚度。一个小圆盘用于在纤维毡的一个相当小的区域上施加一个小的(可重复的)力。一个移动销移动以接触圆盘并完成电路以停止移动并确定圆盘相对于参考平面的位置。通过测量圆盘在有纤维毡和没有纤维毡时与参考平面之间位置的差异来确定纤维毡的厚度。该原型操作简单且用户友好。讨论了该原型的精度和准确性。