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低温熔块釉的应用不会损害 Y-TZP 的疲劳强度。

Low-fusing porcelain glaze application does not damage the fatigue strength of Y-TZP.

机构信息

MSciD and PhD Post-graduate Program in Oral Science, Faculty of Odontology, Federal University of Santa Maria, Santa Maria, Rio Grande do Sul, Brazil.

MSciD Post-graduate Program in Dentistry, School of Dentistry, Meridional Faculty - IMED, Passo Fundo, Rio Grande do Sul, Brazil.

出版信息

J Mech Behav Biomed Mater. 2019 Nov;99:198-205. doi: 10.1016/j.jmbbm.2019.07.022. Epub 2019 Jul 20.

Abstract

This study evaluated and compared the effects of two glaze application methods (brush and spray) on the fatigue strength and surface characteristics (topography and roughness) of a translucent yttrium stabilized partially tetragonal zirconia polycrystal ceramic (Y-TZP) prior to and after grinding. Disc-shaped specimens of translucent Y-TZP (Vita YZ-HT; Vita-Zahnfabrik) were processed (ISO 6872-2015) and randomly allocated into 6 groups, according to the surface treatments performed on the tensile surface: Ctrl - as-sintered (no treatment); Gr - grinding with a diamond bur (181 μm-grit; #3101G); Br - glaze obtained from a powder-liquid mix and applied by brush (Vita Akzent; Vita Zahnfabrik); Sp - glaze application via spray (Vita Akzent Plus; Vita Zahnfabrik); Gr + Br and Gr + Sp - association of grinding + respective glaze method. Analyses of surface roughness (Ra and Rz), fatigue strength (staircase method), surface topography and fractography were carried out. The as-sintered condition had the smoothest surface, while grinding led to the rougher and more heterogeneous topography. Both glaze application methods showed a potential for topography evenness (smoothening effect), while the glaze spray method led to thinner layers of material, showing a limitation in reducing the roughness compared to the brush method. No deleterious effect on fatigue strength of the Y-TZP could be observed, as the glaze-spray application on the as-sintered surface showed the highest values. Fractography depicted two distinct fracture origin regions: from defects in the surface/sub-surface region for the Ctrl and Gr groups; and at the zirconia-glaze layer interface for Br, Sp, Gr + Br and Gr + Sp. The clinical relevance of this work is that the tested glaze application methods did not damage the fatigue strength of the tested Y-TZP.

摘要

本研究评估和比较了两种施釉方法(刷涂和喷涂)对预研磨和研磨后半透明钇稳定部分四方氧化锆多晶陶瓷(Y-TZP)的疲劳强度和表面特性(形貌和粗糙度)的影响。将半透明 Y-TZP(Vita YZ-HT;Vita-Zahnfabrik)的圆盘形试件按拉伸面的表面处理方式随机分组,共 6 组:Ctrl-烧结态(未处理);Gr-金刚石车针研磨(181μm 粒度;#3101G);Br-粉末-液体混合并通过刷涂获得的釉料(Vita Akzent;Vita Zahnfabrik);Sp-通过喷涂进行釉料涂覆(Vita Akzent Plus;Vita Zahnfabrik);Gr+Br 和 Gr+Sp-研磨+相应釉料方法的联合。对表面粗糙度(Ra 和 Rz)、疲劳强度(阶梯法)、表面形貌和断口形貌进行了分析。烧结态的表面最光滑,而研磨导致表面更粗糙且形貌更不均匀。两种施釉方法都具有使形貌均匀的潜力(光滑效果),而釉料喷涂方法导致材料层较薄,与刷涂方法相比,在降低粗糙度方面存在局限性。未观察到对 Y-TZP 疲劳强度的有害影响,因为在烧结态表面上进行的釉料喷涂应用表现出最高的强度值。断口形貌描绘了两个不同的断裂起源区域:对于 Ctrl 和 Gr 组,从表面/次表面区域的缺陷开始;对于 Br、Sp、Gr+Br 和 Gr+Sp 组,在氧化锆-釉层界面处开始。本研究的临床意义在于,所测试的施釉方法未损坏测试的 Y-TZP 的疲劳强度。

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