Jin Limin, Jia Wenbao, Hei Daqian, Zhang Xinlei, Zhao Lei
College of Materials Science and Engineering, Nanjing University of Aeronautics and Astronautics, Nanjing 211106, China.
Rev Sci Instrum. 2019 Aug;90(8):083105. doi: 10.1063/1.5094914.
An energy-selective X-ray tube based on a magnetically controlled method is proposed here. An X-ray tube with two selective targets, modulated by a magnetic field, was developed for the X-ray fluorescence (XRF) analysis of multielement samples. The X-ray tube was small (20 cm length × 4 cm width) and had low power, being operated at 20 W (20 kV, 1 mA). It contained a thermionic cathode and two targets [copper (Cu) and chromium (Cr)] mounted on the anode. The electron beam was drifted by a modulated magnetic field to bombard either the Cu or Cr targets and so produce the required emission spectrum. Particle dynamics analysis software was used to simulate the particle tracking of the X-ray tube. The focal spot on the anode was successfully drifted, and a focal spot at 2 × 2.3 mm was obtained with a pinhole camera method. The XRF analysis of a standard sample (a mixture of FeO and CaCO) was measured by a silicon drift detector. When the bombarding target was changed from Cu to Cr, the characteristic calcium (Ca) X-rays that were detected were twice as strong as those of iron (Fe), but they had a similar excitation efficiency. It was demonstrated that this X-ray tube can provide fast exchangeable X-rays for XRF analysis by modulating the magnetic field intensity and can be further improved by optimizing the structure for alternative applications.
本文提出了一种基于磁控方法的能量选择性X射线管。为了对多元素样品进行X射线荧光(XRF)分析,研制了一种由磁场调制的具有两个选择性靶材的X射线管。该X射线管体积小(长20 cm×宽4 cm)且功率低,工作功率为20 W(20 kV,1 mA)。它包含一个热电子阴极和安装在阳极上的两个靶材[铜(Cu)和铬(Cr)]。电子束通过调制磁场漂移,以轰击Cu靶或Cr靶,从而产生所需的发射光谱。使用粒子动力学分析软件对X射线管的粒子轨迹进行模拟。阳极上的焦点成功漂移,采用针孔相机法获得了2×2.3 mm的焦点。用硅漂移探测器对标准样品(FeO和CaCO的混合物)进行XRF分析。当轰击靶材从Cu变为Cr时,检测到的特征钙(Ca)X射线强度是铁(Fe)的两倍,但它们具有相似的激发效率。结果表明,该X射线管通过调制磁场强度可为XRF分析提供快速可切换的X射线,并且通过优化结构可进一步改进以用于其他应用。