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速度探测器:一种用于高分辨率叠层成像的超快硬X射线纳米探测器。

The Velociprobe: An ultrafast hard X-ray nanoprobe for high-resolution ptychographic imaging.

作者信息

Deng Junjing, Preissner Curt, Klug Jeffrey A, Mashrafi Sheikh, Roehrig Christian, Jiang Yi, Yao Yudong, Wojcik Michael, Wyman Max D, Vine David, Yue Ke, Chen Si, Mooney Tim, Wang Maoyu, Feng Zhenxing, Jin Dafei, Cai Zhonghou, Lai Barry, Vogt Stefan

机构信息

Advanced Photon Source, Argonne National Laboratory, Lemont, Illinois 60439, USA.

School of Chemical, Biological, and Environmental Engineering, Oregon State University, Corvallis, Oregon 97331, USA.

出版信息

Rev Sci Instrum. 2019 Aug;90(8):083701. doi: 10.1063/1.5103173.

DOI:10.1063/1.5103173
PMID:31472643
Abstract

Motivated by the advanced photon source upgrade, a new hard X-ray microscope called "Velociprobe" has been recently designed and built for fast ptychographic imaging with high spatial resolution. We are addressing the challenges of high-resolution and fast scanning with novel hardware designs, advanced motion controls, and new data acquisition strategies, including the use of high-bandwidth interferometric measurements. The use of granite, air-bearing-supported stages provides the necessary long travel ranges for coarse motion to accommodate real samples and variable energy operation while remaining highly stable during fine scanning. Scanning the low-mass zone plate enables high-speed and high-precision motion of the probe over the sample. With an advanced control algorithm implemented in a closed-loop feedback system, the setup achieves a position resolution (3σ) of 2 nm. The instrument performance is evaluated by 2D fly-scan ptychography with our developed data acquisition strategies. A spatial resolution of 8.8 nm has been demonstrated on a Au test sample with a detector continuous frame rate of 200 Hz. Using a higher flux X-ray source provided by double-multilayer monochromator, we achieve 10 nm resolution for an integrated circuit sample in an ultrafast scan with a detector's full continuous frame rate of 3000 Hz (0.33 ms per exposure), resulting in an outstanding imaging rate of 9 × 10 resolution elements per second.

摘要

受先进光子源升级的推动,一种名为“Velociprobe”的新型硬X射线显微镜最近被设计并制造出来,用于具有高空间分辨率的快速叠层成像。我们正在通过新颖的硬件设计、先进的运动控制和新的数据采集策略来应对高分辨率和快速扫描的挑战,包括使用高带宽干涉测量。使用花岗岩、气浮支撑平台为粗运动提供了必要的长行程范围,以适应真实样品和可变能量操作,同时在精细扫描期间保持高度稳定。扫描低质量波带片可使探针在样品上实现高速高精度运动。通过在闭环反馈系统中实施先进的控制算法,该装置实现了2纳米的位置分辨率(3σ)。通过我们开发的数据采集策略,采用二维飞扫叠层成像对仪器性能进行了评估。在金测试样品上,探测器连续帧率为200赫兹时,已证明空间分辨率为8.8纳米。使用双层单色仪提供的更高通量X射线源,在探测器全连续帧率为3000赫兹(每次曝光0.33毫秒)的超快扫描中,我们对集成电路样品实现了10纳米的分辨率,从而实现了每秒9×10分辨率元素的出色成像速率。

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