Jang Yong-Seok, Oh Sang-Hoon, Oh Won-Suck, Lee Min-Ho, Lee Jung-Jin, Bae Tae-Sung
Department of Dental Biomaterials, Institute of Biodegradable Materials, BK21 plus Program, School of Dentistry, Chonbuk National University, Jeonju 54896, Korea.
Haruan Dental Clinic, Department of Dental Biomaterials, Institute of Biodegradable Materials, BK21 plus Program, School of Dentistry, Chonbuk National University, Jeonju 54896, Korea.
Materials (Basel). 2019 Aug 30;12(17):2798. doi: 10.3390/ma12172798.
This study was conducted to test the hypothesis that heat-bonding with a liner positively affects the bond strength and fracture resistance of an implant-supported glass-ceramic crown bonded to a zirconia abutment produced by a computer-aided design/computer-aided milling (CAD/CAM) procedure. Lithium disilicate-reinforced Amber Mill-Q glass ceramic blocks were bonded to 3 mol% yttria stabilized tetragonal zirconia polycrystal (3Y-TZP) blocks by heat-bonding with a liner or cementation with a dual-cure self-adhesive resin cement for a microtensile bond strength test. CAD/CAM implant-supported glass ceramic crowns were produced using Amber Mill-Q blocks and bonded to a milled 3Y-TZP zirconia abutments by heat-bonding or cementation for a fracture test. A statistical analysis was conducted to investigate the significant differences between the experimental results. The mode of failure was analyzed using high-resolution field emission scanning electron microscopy. Chemical bonding was identified at the interface between the zirconia ceramic and liner. The mean tensile bond strength of the liner-bonded group was significantly higher than that of the cement-bonded group. The initial chipping strength of the liner-bonded group was significantly higher than that of the cement-bonded group, although no statistically significant difference was found for the fracture strength. The mode of failure was mixed with cohesive fracture through the liner, whereas the cement-bonded group demonstrated adhesive failure at the interface of bonding.
使用内衬进行热粘结会对通过计算机辅助设计/计算机辅助铣削(CAD/CAM)程序制作的、粘结于氧化锆基台上的种植体支持式玻璃陶瓷冠的粘结强度和抗折性产生积极影响。通过使用内衬进行热粘结或使用双固化自粘结树脂水门汀进行粘结,将硅酸锂增强的Amber Mill-Q玻璃陶瓷块粘结到3 mol%氧化钇稳定的四方多晶氧化锆(3Y-TZP)块上,以进行微拉伸粘结强度测试。使用Amber Mill-Q块制作CAD/CAM种植体支持式玻璃陶瓷冠,并通过热粘结或粘结将其粘结到铣削的3Y-TZP氧化锆基台上,以进行抗折测试。进行统计分析以研究实验结果之间的显著差异。使用高分辨率场发射扫描电子显微镜分析失效模式。在氧化锆陶瓷与内衬之间的界面处鉴定出化学键合。内衬粘结组的平均拉伸粘结强度显著高于水门汀粘结组。内衬粘结组的初始碎裂强度显著高于水门汀粘结组,尽管在抗折强度方面未发现统计学上的显著差异。失效模式为通过内衬的内聚性断裂混合,而水门汀粘结组在粘结界面处表现为粘结性失效。