Post-gel shrinkage, elastic modulus, and stress generated by orthodontic adhesives.

OBJECTIVES

To measure post-gel shrinkage, elastic modulus, and flexural strength of orthodontic adhesives and to predict shrinkage stress using finite element analysis (FEA).

MATERIALS AND METHODS

The following 6 orthodontic adhesives were tested: Transbond XT (3M Unitek, Monrovia, Calif), Transbond Plus Color Change (3M Unitek), Greengloo (Ormco, Brea, Calif), Ortho Connect (GC America, Alsip, Ill), Trulock (RMO, Denver, Colo), GoTo (Reliance, Itasca, Ill). Post-gel shrinkage was measured using a biaxial strain gauge during light curing. Elastic modulus and flexural strength were measured with a 4-point bending test. Analysis of variance and Student-Newman-Keuls post hoc tests were used to compare the shrinkage, elastic modulus, and flexural strengths among the materials (α = .05). Shrinkage stresses caused by the post-gel shrinkage and elastic modulus values were calculated using a cross-sectional FEA of a metallic bracket bonded to an incisor.

RESULTS

Properties were highly different among the adhesives ( ≤ .0001). Transbond XT (0.38 ± 0.09 percent volumetric contraction) and GoTo (0.42 ± 0.05 percent volumetric contraction) had the lowest post-gel shrinkage; Transbond Plus Color Change had the highest (0.84 ± 0.08 percent volumetric contraction). OrthoConnect (6.8 ± 0.6 gigapascals) had the lowest elastic modulus; GoTo (28.3 ± 3.1 gigapascals) had the highest. Trulock (64.1 ± 8.2 megapascals) had the lowest flexural strength; Greengloo (139.1 ± 20.7 megapascals) had the highest. FEA showed that the highest shrinkage stresses were generated with Transbond Plus Color Change and the lowest with OrthoConnect.

CONCLUSIONS

Post-gel shrinkage of orthodontic adhesives was comparable with restorative composites, which are known to create shrinkage stresses in restored teeth. FEA indicated that this shrinkage creates stresses in the adhesive and in the enamel around the brackets.