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[硅胶管中乙二醇样品的研制及其在实验室间比对中的应用]

[Development of ethylene glycol Samples in silicone tubes and their application in inter-laboratory comparison].

作者信息

Pan Y J, Zhang J, Pan X F, Yan H F

机构信息

National Institute of Occupational Health and Poison Control, Beijing 100050, China.

出版信息

Zhonghua Lao Dong Wei Sheng Zhi Ye Bing Za Zhi. 2019 Sep 20;37(9):714-717. doi: 10.3760/cma.j.issn.1001-9391.2019.09.021.

Abstract

To development of ethylene glycol samples in silicone tubes, and the samples were applied to inter-laboratory comparison, through it to evaluate the detection capacity of occupational health testing laboratories. Three content levels of ethylene glycol samples in silicone tubes were prepared, and the homogeneity and stability of samples were investigated, the results were statistically analyzed. A robust statistical four-point distance method was used to calculate the results submitted by each participant laboratory and the test capability of the laboratory was assessed by the z-score method. The statistic of the homogeneity of ethylene glycol samples in silicone tubes were less than the critical value (>0.05) , and the samples were stable at room temperature for one month. The satisfactory rate of comparison between 204 laboratories was 88.24%. The homogeneity and stability of the ethylene glycol samples in the silicone tubes can meet the requirements of proficiency testing and can be used for laboratory comparison. Most of the laboratories that participated in the comparison had the ability to detect ethylene glycol.

摘要

制备了硅胶管中乙二醇样品用于实验室间比对,通过该比对评估职业健康检测实验室的检测能力。制备了硅胶管中三种含量水平的乙二醇样品,研究了样品的均匀性和稳定性,并对结果进行统计分析。采用稳健统计四点距离法计算各参与实验室提交的结果,并用z分数法评估实验室的检测能力。硅胶管中乙二醇样品均匀性统计值小于临界值(>0.05),且样品在室温下稳定一个月。204家实验室比对满意率为88.24%。硅胶管中乙二醇样品的均匀性和稳定性能够满足能力验证要求,可用于实验室间比对。参与比对的大多数实验室具备检测乙二醇的能力。

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