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[生活饮用水中氟化物测定能力验证]

[Proficiency test for determination of fluoride in drinking water].

作者信息

Yang Jiaolan, Cao Ningtao

机构信息

National Institute of Environmental Health, Chinese Center for Disease Control and Prevention, Beijing 100021, China.

出版信息

Wei Sheng Yan Jiu. 2019 Sep;48(5):838-842.

Abstract

OBJECTIVE

To evaluate the capacity of national laboratories for determination of fluoride in drinking water using proficiency testing program.

METHODS

The preparation method of the secondary standard materials were used as the reference for the sample preparation in this proficiency testing program. The homogeneity and stability of the samples were tested by single factor analysis of variance( ANOVA) and linear regression. The results provided by participant laboratories were analyzed by robust statistics and assessed using the Z-score.

RESULTS

A total of 985 laboratories throughout the country participated in the proficiency testing program. 910 laboratories, or92. 4% of total participating laboratories, obtained satisfactory result. Results provided by26 laboratories, or 2. 6% of total participating laboratories, were found to suggest doubts in their capacities. Finally, there were 49 laboratories, constituting 5. 0% of total participating laboratories, with results that were found to be outliers.

CONCLUSION

The capacity of national laboratories for determination of fluoride in drinking water has been ranked as satisfactory according to statistical analysis of the proficiency testing program results. Only a small portion of the participants require further improvement in their capacities.

摘要

目的

利用能力验证计划评估国家实验室测定饮用水中氟化物的能力。

方法

在本次能力验证计划中,以二级标准物质的制备方法作为样品制备的参考。通过单因素方差分析(ANOVA)和线性回归对样品的均匀性和稳定性进行测试。采用稳健统计分析参与实验室提供的结果,并使用Z分数进行评估。

结果

全国共有985家实验室参加了能力验证计划。910家实验室(占参与实验室总数的92.4%)获得了满意结果。26家实验室(占参与实验室总数的2.6%)提供的结果表明其能力存疑。最后,有49家实验室(占参与实验室总数的5.0%)的结果被认定为异常值。

结论

根据能力验证计划结果的统计分析,国家实验室测定饮用水中氟化物的能力被评定为满意。只有一小部分参与者需要进一步提高其能力。

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