Cao Ningtao, Yang Jiaolan
National Institute of Environmental Health Chinese Center for Disease Control and Prevention, Beijing 100021, China.
Wei Sheng Yan Jiu. 2020 Jul;49(4):630-634. doi: 10.19813/j.cnki.weishengyanjiu.2020.04.020.
To evaluate the capacity of national laboratories for determination of chlorate in drinking water using Proficiency Testing Program.
The preparation method of the Secondary Standard Materials were used as the reference for the sample preparation in this Proficiency Testing Program. The homogeneity and stability of the samples and short-term stability for simulated transportation were tested by Single Factor Analysis of Variance(ANOVA) and Linear Regression and Mean consistency test. The result provided by participant laboratories were analyzed by robust statistics and assessed using the Z-score.
A total of 327 laboratories throughout the country participated in the Proficiency Testing Program. 307 laboratories, or 93. 9% of total participating laboratories, obtained satisfactory result. Results provided by 5 laboratories, or 1. 5% of total participating laboratories, were found to suggest doubts in their capacities. Finally, there were 15 laboratories, constituting 4. 6% of total participating laboratories, with result that were found to be outliers.
The capacity of national laboratories for determination of chlorate in drinking water has been ranked as satisfactory according to statistical analysis of the Proficiency Testing Program result. Only a small portion of the participants require further improvement in their capacities.
通过能力验证计划评估国家实验室测定饮用水中氯酸盐的能力。
本能力验证计划中样品制备以二级标准物质的制备方法为参考。采用单因素方差分析(ANOVA)、线性回归和均值一致性检验对样品的均匀性、稳定性以及模拟运输的短期稳定性进行测试。采用稳健统计方法分析参与实验室提供的结果,并使用Z分数进行评估。
全国共有327家实验室参与了该能力验证计划。307家实验室(占参与实验室总数的93.9%)获得了满意结果。5家实验室(占参与实验室总数的1.5%)提供的结果表明其能力存疑。最后,有15家实验室(占参与实验室总数的4.6%)的结果被判定为离群值。
根据能力验证计划结果的统计分析,国家实验室测定饮用水中氯酸盐的能力评定为满意。只有一小部分参与者需要进一步提高其能力。