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超微粉碎对消旋山莨菪碱粉末中鳞茎理化性质的影响。

Effect of superfine grinding on the physicochemical properties of bulbs of Hsiao et K.C. Hsia powder.

作者信息

Li Cai-Xia, Liu Ying-Ying, Feng Hai-Sheng, Ma Shi-Zhen

机构信息

Northwest Institute of Plateau Biology Chinese Academy of Sciences Xining China.

Qinghai Provincial Key Laboratory of Qinghai-Tibet Plateau Biological Resources Xining China.

出版信息

Food Sci Nutr. 2019 Sep 13;7(11):3527-3537. doi: 10.1002/fsn3.1203. eCollection 2019 Nov.

Abstract

This work aimed to determine the influence of superfine grinding on the physicochemical properties of bulbs of Hsiao et K.C. Hsia (BFU) powder. For this purpose, fine powder (FP) and two superfine powders (SPs) were obtained via superfine and conventional grinding methods. The properties of different powders were studied and compared. Compared with FP, SPs exhibited higher values in terms of the angle of repose, swelling capacity, ethanol extraction yield, total alkaloid content, and imperialine content, while lower values in terms of particle size and bulk density. Especially, the total alkaloid content of SP-I increased by 66.7%. Proper grinding is more conducive to reduce particle size and improve alkaloid content. FTIR analysis indicates that no new functional groups produced after superfine grinding. XRD analysis suggests that grinding treatment lead to decreases in the crystallinity. Therefore, superfine grinding displays immense potential in the BFU application.

摘要

本研究旨在确定超微粉碎对小(Hsiao)贝母(BFU)鳞茎粉末理化性质的影响。为此,通过超微粉碎和传统粉碎方法分别制备了细粉(FP)和两种超微粉(SPs)。对不同粉末的性质进行了研究和比较。与FP相比,SPs的休止角、溶胀度、乙醇提取物得率、总生物碱含量和贝母素甲含量更高,而粒径和堆密度更低。特别是,SP-I的总生物碱含量提高了66.7%。适当的粉碎更有利于减小粒径并提高生物碱含量。傅里叶变换红外光谱(FTIR)分析表明,超微粉碎后未产生新的官能团。X射线衍射(XRD)分析表明,粉碎处理导致结晶度降低。因此,超微粉碎在BFU应用中显示出巨大潜力。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1b6a/6848833/6a631a4f509a/FSN3-7-3527-g001.jpg

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