State Key Laboratory for Manufacturing Systems Engineering, Xi'an Jiaotong University, Xi'an, Shaanxi, 710049, People's Republic of China.
Nanotechnology. 2020 Apr 3;31(14):145707. doi: 10.1088/1361-6528/ab6239. Epub 2019 Dec 16.
Carbon nanotube (CNT) probes are used in atomic force microscopes (AFMs) for high-resolution imaging, especially in the measurement of high aspect ratio micro/nano structures. Due to the use of a longer CNT tip leading to the degradation of image resolution, researchers have used several methods to cut CNTs. However, the principle of the selection of the cutting length has hardly been reported. Moreover, the influence of the effect of size on the mechanical properties of a CNT tip is not fully understood. In this study, an accurate model of finite element simulations is constructed on the basis of scanning electron microscopy data to investigate the mechanical properties of a CNT probe. An elastic model is employed to study the factors that influence the critical buckling force at the CNT tip during the measurement process. The calculation shows that the mechanical stiffness of the probe is affected by the diameter and the length-to-diameter ratio of the CNT tip. The changes in the von Mises stress at the bond between the AFM probe and the CNT tip as well as the variation of the strain energy at the CNT tip are discussed. It is hoped that this study will provide guidance for the selection of the cutting length of CNT-AFM probes and propose a basis for probe selection and design in practical measurements.
碳纳米管 (CNT) 探针用于原子力显微镜 (AFM) 进行高分辨率成像,特别是在测量高纵横比微/纳米结构时。由于使用较长的 CNT 尖端会导致图像分辨率降低,因此研究人员已经使用了几种方法来切割 CNT。然而,几乎没有报道过选择切割长度的原理。此外,对于 CNT 尖端的尺寸对机械性能的影响也没有完全理解。在这项研究中,基于扫描电子显微镜数据构建了一个精确的有限元模拟模型,以研究 CNT 探针的机械性能。采用弹性模型研究了在测量过程中影响 CNT 尖端临界屈曲力的因素。计算表明,探针的机械刚度受 CNT 尖端的直径和长径比的影响。讨论了 AFM 探针和 CNT 尖端之间的键合处的 von Mises 应力变化以及 CNT 尖端处应变能的变化。希望本研究能够为 CNT-AFM 探针的切割长度选择提供指导,并为实际测量中的探针选择和设计提供依据。