Department and Research Institute of Dental Biomaterials and Bioengineering, Yonsei University College of Dentistry, Seoul, Republic of Korea.
Department of Orthopedic Surgery, Columbia University, New York, NY, USA.
Dent Mater. 2020 Apr;36(4):e117-e125. doi: 10.1016/j.dental.2020.01.014. Epub 2020 Feb 5.
This study evaluates the difference in physical and mechanical properties of ZrO ceramics, commonly used in dental applications, altered by three different forms of AlO content; microparticles (m), nanoparticles (n), and microfiber (f).
Three different types of ZrO-AlO composites were formed using microparticle (m), nanoparticle (n), or microfibre (f) forms of AlO. The physical and mechanical properties such as sintering shrinkage, relative density, Vickers hardness, fracture toughness, and biaxial strength were evaluated. A Weibull analysis was performed to assess the strength reliability of the specimens. All data were calculated using the t-test and ANOVA.
The sintering shrinkage and relative density of all ceramic composite groups were decreased with the addition of AlO. The mechanical properties of ZrO-AlO (f) composite were higher than that of ZrO-AlO (m) composite and ZrO-AlO (n) composite. The maximum hardness, fracture toughness, and biaxial flexural strength were observed for 10 vol% of AlO fibre. When the content of AlO fibre in the matrix was increased above 20 vol%, agglomeration occurred and resulted in a decrease of hardness and toughness. The Weibull modulus value of the ZrO-AlO (f) composite was the lowest compared to that of other groups. However, characteristic strength (σ) of ZrO-AlO (f) the highest value.
The current study demonstrated that the addition of right amount of AlO microfibre into the ZrO matrix enhanced the mechanical properties of ZrO-AlO (f) composite, which would be favourable for dental applications.
本研究评估了在牙科应用中常用的氧化锆陶瓷(ZrO),经三种不同形式的氧化铝(AlO)含量改变后,其物理和机械性能的差异。
使用 AlO 的微粒(m)、纳米粒子(n)或微纤维(f)三种不同形式形成三种不同类型的 ZrO-AlO 复合材料。评估了烧结收缩率、相对密度、维氏硬度、断裂韧性和双轴强度等物理和机械性能。进行了威布尔分析以评估样品的强度可靠性。所有数据均使用 t 检验和 ANOVA 进行计算。
所有陶瓷复合材料组的烧结收缩率和相对密度随 AlO 的加入而降低。ZrO-AlO(f)复合材料的机械性能高于 ZrO-AlO(m)复合材料和 ZrO-AlO(n)复合材料。观察到 10vol% AlO 纤维时,硬度、断裂韧性和双轴弯曲强度达到最大值。当基体中 AlO 纤维的含量增加到 20vol%以上时,会发生团聚,导致硬度和韧性下降。与其他组相比,ZrO-AlO(f)复合材料的威布尔模数值最低。然而,ZrO-AlO(f)的特征强度(σ)值最高。
本研究表明,适量 AlO 微纤维添加到 ZrO 基体中增强了 ZrO-AlO(f)复合材料的机械性能,这将有利于牙科应用。