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花生油饼衍生纤维素纤维:提取、机械和热性能在菠萝/亚麻天然纤维复合材料中的应用。

Peanut oil cake-derived cellulose fiber: Extraction, application of mechanical and thermal properties in pineapple/flax natural fiber composites.

机构信息

Department of Mechanical Engineering, Anna University Regional Campus, Coimbatore 641046, Tamilnadu, India.

Department of Mechanical Engineering, Karpagam Academy of Higher Education, Coimbatore 641 021, Tamilnadu, India.

出版信息

Int J Biol Macromol. 2020 May 1;150:775-785. doi: 10.1016/j.ijbiomac.2020.02.118. Epub 2020 Feb 12.

Abstract

In this work peanut oil cake extracted Cellulose Micro Filler (CMF) is used for the advancement of mechanical and thermal properties in natural fiber composites. This fiber powder was used in enhancing the applications of Pineapple (P)/Flax (F) natural fiber epoxy composites. The X Ray Diffraction (XRD) results of CMF showed improved Crystalline Index (Crl) of 70.25° and crystalline size of 5.5 nm. FTIR results confirmed the rich cellulose content in functional groups of filler with peaks at 1058 cm, 1162 cm, 1370 cm and 1428 cm. Mechanical results showed a positive impact with incorporation of CMF in PF hybrid fiber composites. Thermal stability results showed enhancement in the degradation temperature, residual %, endothermic peak and enthalpy by the incorporation of CMF. In the 30% PF combinations degradation temperature T, T, T enhanced from 387.73-391.08°, 434.81-454.81° and 468.91-553.36° by the filler substitution. Similarly residual % increased from 17.69-24.35%. The combination with 35% PF showed enhancement in degradation temperature, residual percentage, endothermic peak and enthalpy with filler addition up to 3%.

摘要

在这项工作中,使用花生油提取的纤维素微填料(CMF)来提高天然纤维复合材料的机械和热性能。这种纤维粉末用于增强菠萝(P)/亚麻(F)天然纤维环氧复合材料的应用。CMF 的 X 射线衍射(XRD)结果表明,结晶指数(Crl)提高到 70.25°,结晶尺寸为 5.5nm。傅里叶变换红外(FTIR)结果证实了填料中纤维素含量丰富,在 1058cm、1162cm、1370cm 和 1428cm 处有峰。力学结果表明,在 PF 混合纤维复合材料中加入 CMF 有积极的影响。热稳定性结果表明,通过加入 CMF,降解温度、残余%、吸热峰和焓值都得到了提高。在 30%PF 组合中,降解温度 T、T、T 分别从 387.73-391.08°C、434.81-454.81°C 和 468.91-553.36°C 通过填料取代得到提高。同样,残余%从 17.69%-24.35%增加。在添加 3%的填料时,与 35%PF 的组合在降解温度、残余百分比、吸热峰和焓值方面都得到了提高。

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