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添加 Al 和造孔剂含量对用于骨支架的 Ti2Co 合金泡沫微观结构和力学性能的影响。

Effect of Al addition and space holder content on microstructure and mechanical properties of Ti2Co alloys foams for bone scaffold application.

机构信息

AcSIR AMPRI (Academy of Scientific & Innovative Research - Advanced Materials and Processes Research Institute), Bhopal 462026, India.

AcSIR AMPRI (Academy of Scientific & Innovative Research - Advanced Materials and Processes Research Institute), Bhopal 462026, India.

出版信息

Mater Sci Eng C Mater Biol Appl. 2020 Apr;109:110600. doi: 10.1016/j.msec.2019.110600. Epub 2020 Jan 2.

Abstract

Ti2Co alloy (with and without Al) foam of varying densities were prepared through space holder technique, in which space holder varied from 40 to 70 vol% and Al-concentration varied from 0 to 6 wt% with an enhancement of 2 wt%. The prepared foam samples were analysed in terms of microstructure, phase analysis and mechanical properties. The sizes of pores in the foams come to be almost similar to that of space holder. An increase in the amount of Al resulted in enhancement of the mechanical properties such as comprehensive strength, plateau stress, energy absorption capacity, hardness and Young's modulus due to increase in solid solution strengthening and variation in morphology of eutectoid phase. Also, these values are found to be predictable with the generalized relation through adjustment of the fraction of materials at cell edges and cell walls. The openness of the investigated foams was calculated to obtain degree of openness. The corrosion rate was calculated for each sample of Ti2Co alloys foams and compared with the reported values. The microstructure and mechanical properties of the prepared foams were also compared with that of the human bone.

摘要

采用造孔剂法制备了不同密度的 Ti2Co 合金(含 Al 和不含 Al)泡沫,造孔剂体积分数为 40%70%,Al 浓度为 06wt%,每增加 2wt%。对制备的泡沫样品进行了微观结构、相分析和力学性能分析。泡沫中的孔径大小几乎与造孔剂相同。随着 Al 含量的增加,由于固溶强化的增加和共析相形态的变化,力学性能如综合强度、平台应力、能量吸收能力、硬度和杨氏模量得到提高。此外,通过调整胞壁和胞壁边缘材料的分数,这些值可以通过广义关系进行预测。计算了所研究泡沫的开口度以获得开口度。计算了每个 Ti2Co 合金泡沫样品的腐蚀速率,并与报道的值进行了比较。还将制备的泡沫的微观结构和力学性能与人体骨骼进行了比较。

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