Bae Byeong Hoon, Lee Jeong Woo, Cha Jae Min, Kim Il-Won, Jung Hyun-Do, Yoon Chang-Bun
Department of Advanced Materials Engineering, Korea Polytechnic University, Siheung-si 15073, Korea.
Department of BioMedical-Chemical Engineering (BMCE), The Catholic University of Korea, Bucheon 14662, Korea.
Materials (Basel). 2020 May 7;13(9):2156. doi: 10.3390/ma13092156.
Powder bed fusion (PBF) additive manufacturing (AM) is currently used to produce high-efficiency, high-density, and high-performance products for a variety of applications. However, existing AM methods are applicable only to metal materials and not to high-melting-point ceramics. Here, we develop a composite material for PBF AM by adding AlO to a glass material using laser melting. AlO and a black pigment are added to a synthesized glass frit for improving the composite strength and increased laser-light absorption, respectively. Our sample analysis shows that the glass melts to form a composite when the mixture is laser-irradiated. To improve the sintering density, we heat-treat the sample at 750 °C to synthesize a high-density glass frit composite. As per our X-ray diffraction (XRD) analysis to confirm the reactivity of the glass frit and AlO, we find that no reactions occur between glass and crystalline AlO. Moreover, we obtain a high sample density of ≥95% of the theoretical density. We also evaluate the composite's mechanical properties as a function of the AlO content. Our approach facilitates the manufacturing of ceramic 3D structures using glass materials through PBF AM and affords the benefits of reduced process cost, improved performance, newer functionalities, and increased value addition.
粉末床熔融(PBF)增材制造(AM)目前用于生产适用于各种应用的高效、高密度和高性能产品。然而,现有的增材制造方法仅适用于金属材料,不适用于高熔点陶瓷。在此,我们通过激光熔化将AlO添加到玻璃材料中,开发了一种用于PBF增材制造的复合材料。分别向合成的玻璃料中添加AlO和黑色颜料,以提高复合材料强度和增加激光吸收。我们的样品分析表明,当混合物受到激光照射时,玻璃会熔化形成复合材料。为了提高烧结密度,我们在750℃对样品进行热处理,以合成高密度玻璃料复合材料。根据我们用于确认玻璃料与AlO反应性的X射线衍射(XRD)分析,我们发现玻璃与结晶AlO之间不发生反应。此外,我们获得了高达理论密度95%的高样品密度。我们还评估了复合材料的机械性能与AlO含量的关系。我们的方法有助于通过PBF增材制造使用玻璃材料制造陶瓷三维结构,并带来降低工艺成本、提高性能、增加新功能和附加值的好处。