J Adhes Dent. 2020;22(3):311-320. doi: 10.3290/j.jad.a44554.
To evaluate the effects of double application of resin cement primers to dentin prepared with different diamond burs on the cement-dentin bond strengths.
Sixty flat dentin surfaces were prepared and divided into 12 groups (n = 5) according to three experimental factors: 1. resin cements: RelyX Ultimate (RU), Multilink Automix (ML), and Panavia V5 (PV); 2. resin cement primer application: single or double; 3. dentin surface preparation with regular or superfine diamond burs. Cement-dentin sticks (1 mm2) were prepared for and underwent microtensile bond strength testing (µTBS). Statistical analysis was performed using three-way ANOVA and Duncan's test (α = 0.05). Fractured surfaces and cement-dentin interfaces were observed using SEM. Additional teeth were used to observe the demineralization effect of resin cement primers with SEM and transmission electron microscopy (TEM).
All tested factors demonstrated significant effects on µTBS (p < 0.001). The combination of PV with superfine-grit bur and double application yielded the highest bond strengths. Surfaces prepared with superfine-grit burs demonstrated higher µTBS than did the regular-grit group, but a significant effect was not observed for all groups. The double application of primer significantly increased the bond strength for most combinations, except for PV with superfine-grit bur-prepared dentin.
PV showed higher bond strengths than other resin cements. Double application of primer improved the bond strength of all cements to dentin. Bond strengths were higher when dentin was prepared with a superfine-grit bur.
评估不同金刚石钻头制备的牙本质表面双次应用树脂粘结剂底漆对粘结剂-牙本质粘结强度的影响。
制备 60 个牙本质平面表面,并根据三个实验因素分为 12 组(n = 5):1. 树脂粘结剂:RelyX Ultimate(RU)、Multilink Automix(ML)和 Panavia V5(PV);2. 树脂粘结剂底漆应用:单次或双次;3. 常规或超细金刚石钻头制备的牙本质表面。制备粘结剂-牙本质棒(1mm2)并进行微拉伸粘结强度测试(µTBS)。使用三因素方差分析和 Duncan 检验(α = 0.05)进行统计分析。使用扫描电子显微镜(SEM)观察断裂表面和粘结剂-牙本质界面。使用 SEM 和透射电子显微镜(TEM)观察树脂粘结剂底漆的脱矿作用。
所有测试因素均对 µTBS 有显著影响(p < 0.001)。PV 与超细粒度钻头结合并双次应用时产生最高的粘结强度。与常规粒度组相比,使用超细粒度钻头制备的表面具有更高的 µTBS,但并非所有组均观察到显著效果。除了 PV 与超细粒度钻头制备的牙本质外,底漆的双次应用显著提高了大多数组合的粘结强度。
PV 显示出比其他树脂粘结剂更高的粘结强度。底漆的双次应用提高了所有粘结剂与牙本质的粘结强度。使用超细粒度钻头制备牙本质时,粘结强度更高。