Poryles Raphaël, Gland Nicolas, King Andrew, Rosenberg Elisabeth, Barré Loïc, Chevalier Thibaud
IFP Energies nouvelles, 1 et 4 avenue de Bois-Préau, 92852 Rueil-Malmaison, France.
Synchrotron SOLEIL, 91192 Saint-Aubin, France.
Soft Matter. 2020 Jul 15;16(27):6354-6361. doi: 10.1039/d0sm00392a.
One of the challenges in the study of foam transport in 3D porous media is to have an adequate spatial and temporal resolution to get a better understanding of the local phenomenon at the pore scale in a non-destructive way. We present an experimental study in which ultra-fast X-ray microtomography is used to investigate the foam trapping while the foam is flowing in a 3D porous medium. Preformed aqueous foam is injected into a rotating cell containing a 3D granular medium made of silica grains. The use of rotating seals allows the cell to rotate continuously at a rate of one revolution per second, compatible with the fast X-ray tomography at SOLEIL synchrotron. We visualize the foam flow and track the trapping of bubbles with an acquisition time of about one second and a spatial resolution of a few microns (pixel size of one micron). This allows us to extract the characteristics and reliable statistics about trapped bubbles inside the granular medium and to observe their local behavior. With this setup and technique we obtain access to the dynamics of foam trapping during the flow and the texture variations of the foam in the trapped zones. These local trapping events are well correlated with the macroscopical measurement of the pressure gradient over the cell.
三维多孔介质中泡沫传输研究的挑战之一是要有足够的空间和时间分辨率,以便以非破坏性方式更好地理解孔隙尺度上的局部现象。我们开展了一项实验研究,其中使用超快速X射线显微断层扫描技术来研究泡沫在三维多孔介质中流动时的捕集情况。将预制的水性泡沫注入到一个旋转单元中,该单元包含由硅颗粒制成的三维颗粒介质。旋转密封的使用使得该单元能够以每秒一转的速度连续旋转,这与SOLEIL同步加速器的快速X射线断层扫描兼容。我们以大约一秒的采集时间和几微米的空间分辨率(像素大小为一微米)来可视化泡沫流动并跟踪气泡的捕集情况。这使我们能够提取颗粒介质内捕获气泡的特征和可靠统计数据,并观察它们的局部行为。通过这种设置和技术,我们能够了解流动过程中泡沫捕集的动力学以及捕集区域内泡沫的纹理变化。这些局部捕集事件与单元上压力梯度的宏观测量结果密切相关。