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旋转锻造后W/Ni-Co复合材料的织构与差应力发展

Texture and Differential Stress Development in W/Ni-Co Composite after Rotary Swaging.

作者信息

Strunz Pavel, Kocich Radim, Canelo-Yubero David, Macháčková Adéla, Beran Přemysl, Krátká Ludmila

机构信息

Nuclear Physics Institute of the CAS, Řež 130, 25068 Řež, Czech Republic.

Faculty of Materials Science and Technology, VŠB-Technical University of Ostrava, 708 00 Ostrava, Czech Republic.

出版信息

Materials (Basel). 2020 Jun 26;13(12):2869. doi: 10.3390/ma13122869.

Abstract

Knowledge of texture and residual stresses in tungsten heavy pseudoalloys is substantial for the microstructure optimization. These characteristics were determined in cold and warm rotary swaged W/NiCo composite with help of neutron diffraction. The results were discussed in view of the observed microstructure and mechanical properties. The investigated bars consisted of tungsten agglomerates (bcc lattice) surrounded by NiCo-based matrix (fcc lattice). No preferential crystallographic orientation was found in the as-sintered bar. A strong texture was formed in both the tungsten agglomerates (<101> fiber texture parallel to the swaging axis) and in the NiCo-based matrix (<111> fiber texture) after rotary swaging. Although usually of double-fiber texture, the <001> fiber of the fcc structures was nearly missing in the matrix. Further, the cold-swaged bar exhibited substantially stronger texture for both phases which corresponds to the higher measured ultimate tensile strength. The residual stress differences were employed for characterization of the stress state of the bars. The largest residual stress difference (≈400 MPa) was found at the center of the bar deformed at room temperature. The hoop stresses were non-symmetrical with respect to the swaging axis, which was likely caused by the elliptical cross section of the as-sintered bar.

摘要

了解钨基重质假合金中的织构和残余应力对于微观结构优化至关重要。借助中子衍射确定了冷旋压和温旋压W/NiCo复合材料中的这些特性。结合观察到的微观结构和力学性能对结果进行了讨论。所研究的棒材由被NiCo基基体(面心立方晶格)包围的钨团聚体(体心立方晶格)组成。烧结态棒材中未发现择优结晶取向。旋压后,钨团聚体(<101>纤维织构平行于旋压轴)和NiCo基基体(<111>纤维织构)中均形成了强烈的织构。尽管通常为双纤维织构,但面心立方结构的<001>纤维在基体中几乎缺失。此外,冷旋压棒材的两个相均表现出明显更强的织构,这与测得的更高极限抗拉强度相对应。利用残余应力差异来表征棒材的应力状态。在室温下变形的棒材中心发现了最大的残余应力差异(约400MPa)。环向应力相对于旋压轴不对称,这可能是由于烧结态棒材的椭圆形横截面所致。

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