在有和没有南极假丝酵母脂肪酶B的情况下核糖-油酸酯的合成
Synthesis of Ribose - Oleic Acid Esters in the Presence- and Absence of Candida antarctica Lipase B.
作者信息
Çetinkaya Serap, Yenidünya Ali Fazıl, Başoğlu Faika, Saraç Kamuran
机构信息
Department of Molecular Biology and Genetics, Science Faculty, Sivas Cumhuriyet University.
Department of Pharmaceutical Chemistry, Faculty of Pharmacy, Europen University of Lefke.
出版信息
J Oleo Sci. 2020 Aug 6;69(8):907-912. doi: 10.5650/jos.ess20086. Epub 2020 Jul 9.
D-ribose-oleic acid esters were produced with or without a biocatalyst, using in the same organic media, dimethyl sulfoxide (DMSO): tert-butanol (TBU) or 2-methyl-2-butanol (2M2B). The yield of the ester product was above 90% in both of the reactions. The biocatalyst used was lipase B of Candida antarctica. Molecular characterization was performed by using all the analytical methods available: IR, H-NMR and C-NMR, HSQC, and ESI-MS.
在有或没有生物催化剂的情况下，于相同有机介质二甲基亚砜（DMSO）：叔丁醇（TBU）或2-甲基-2-丁醇（2M2B）中制备D-核糖油酸酯。两个反应中酯产物的产率均高于90%。所使用的生物催化剂是南极假丝酵母脂肪酶B。通过使用所有可用的分析方法进行分子表征：红外光谱（IR）、氢核磁共振（H-NMR）和碳核磁共振（C-NMR）、异核单量子相干谱（HSQC）以及电喷雾电离质谱（ESI-MS）。
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