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面包果OSA淀粉和表面活性剂在利用高压均质化和低频超声处理稳定高油负载乳液中的作用。

The role of breadfruit OSA starch and surfactant in stabilizing high-oil-load emulsions using high-pressure homogenization and low-frequency ultrasonication.

作者信息

Anwar Sri Haryani, Hasni Dian, Rohaya Syarifah, Antasari Miranda, Winarti Christina

机构信息

Department of Agricultural Product Technology, Universitas Syiah Kuala, Banda Aceh 23111, Indonesia.

Indonesian Center for Agricultural Postharvest Research and Development-IAARD, Jalan Tentara Pelajar No. 12, Bogor, West Java, Indonesia.

出版信息

Heliyon. 2020 Jul 4;6(7):e04341. doi: 10.1016/j.heliyon.2020.e04341. eCollection 2020 Jul.

Abstract

This study aimed to investigate the role of modified breadfruit starch in the presence of Tween 80 for stabilizing the oil-in-water emulsions. An ultra turrax homogenizer was used to produce coarse emulsions, followed by high-pressure homogenization (HPH) or low-frequency ultrasonication (LFU) for fine emulsions. The breadfruit starch was chemically modified using octenyl succinic anhydride (OSA) to produce modified breadfruit OSA starch (BOSA). The dispersed phase was a mixture of palm and lemon oil in a 9:1 ratio. Two BOSA (1% and 2%), three oil concentrations (10%, 25%, and 40%) and Tween 80 (1% of the total amount of oil) were examined based on the emulsion stability. The Fourier transform infrared spectroscopy (FTIR) indicated that starch modification was successful (Degree of Substitution-DS, 0.0241). The most stable coarse emulsions contained 40% oil and 2% BOSA starch. The same formula produced fine emulsions that remained stable for over 42 days, regardless of the homogenization method. BOSA starch and Tween 80 exhibit a mixed stabilization effect on the oil-in-water emulsions. HPH produced more uniformly sized emulsion droplets when compared with those produced using LFU.

摘要

本研究旨在探讨改性面包果淀粉在吐温80存在下对水包油乳液的稳定作用。使用超高速均质机制备粗乳液,然后通过高压均质化(HPH)或低频超声处理(LFU)制备细乳液。面包果淀粉用辛烯基琥珀酸酐(OSA)进行化学改性,以制备改性面包果OSA淀粉(BOSA)。分散相是棕榈油和柠檬油按9:1比例混合而成。基于乳液稳定性,考察了两种BOSA(1%和2%)、三种油浓度(10%、25%和40%)以及吐温80(占油总量的1%)。傅里叶变换红外光谱(FTIR)表明淀粉改性成功(取代度-DS,0.0241)。最稳定的粗乳液含有40%的油和2%的BOSA淀粉。无论采用何种均质方法,相同配方制备的细乳液在42天以上均保持稳定。BOSA淀粉和吐温80对水包油乳液具有混合稳定作用。与使用LFU制备的乳液滴相比,HPH制备的乳液滴尺寸更均匀。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/6c7e/7339058/fb040d68bb69/gr1.jpg

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