Department of Chemical and Environmental Engineering, University of Oviedo, Julián Clavería 8, 33006 Oviedo, Spain.
Department of Food Technology, Engineering, and Nutrition, Lund University, P.O. Box 124, SE 221 00 Lund, Sweden.
Food Res Int. 2021 Jan;139:109837. doi: 10.1016/j.foodres.2020.109837. Epub 2020 Oct 27.
Resveratrol is a photosensitive, bioactive molecule which has received increasing research interest during the past decade for its antioxidant properties. However, it has low solubility in water or common triglyceride oils. Resveratrol solubilization in oil can only be achieved in essential oils, such as flavour oils, but the stability of emulsions produced with this type of oils is low as they are prone to creaming phenomena and Oswald ripening. In this study, resveratrol was first dissolved in orange oil which was mixed into a medium-chain triglyceride (Miglyol) at different ratios and used as the internal phase of oil-in-water emulsions (O/W). The emulsions were stabilized by octenyl succinic anhydride (OSA) modified rice starch granules using two different ratios of starch particle:oil to study the influence of interfacial coverage on the final emulsion droplet size and emulsion stability. The results of this study indicated that stable Pickering emulsions could be prepared using OSA-modified rice starch granules even at partial coverage conditions. Emulsions prepared at an oil fraction of 0.5 using 30% v/v mixture of orange oil in Miglyol as the dispersed phase seemed to be an appropriate resveratrol carrier system, obtaining encapsulation efficiency values close to 90% which results in emulsions with a resveratrol concentration of 8.45 mg/L. Hence, the emulsions prepared are suitable for food fortification applications.
白藜芦醇是一种感光、生物活性分子,由于其抗氧化特性,在过去十年中受到越来越多的研究关注。然而,它在水中或常见的甘油三酯油中的溶解度很低。白藜芦醇在油中的溶解只能在精油中实现,如调味油,但这种油制成的乳液稳定性较低,因为它们容易出现乳状液分层和奥斯特瓦尔德熟化现象。在这项研究中,白藜芦醇首先溶解在橙油中,然后将其以不同的比例混入中链甘油三酯(Miglyol)中,并用作水包油(O/W)乳液的内相。用两种不同的淀粉颗粒与油的比例,用辛烯基琥珀酸酐(OSA)改性的大米淀粉颗粒来稳定乳液,研究界面覆盖度对最终乳液液滴大小和乳液稳定性的影响。研究结果表明,即使在部分覆盖的条件下,也可以使用 OSA 改性的大米淀粉颗粒制备稳定的 Pickering 乳液。在油分数为 0.5 的条件下,使用 30%v/v 的橙油和 Miglyol 的混合物作为分散相制备的乳液似乎是一种合适的白藜芦醇载体系统,可获得接近 90%的包封效率值,这使得乳液中白藜芦醇的浓度达到 8.45mg/L。因此,所制备的乳液适用于食品强化应用。