Malla Komal Prasad, Regmi Sagar, Nepal Achyut, Bhattarai Sitaram, Yadav Ram Jeewan, Sakurai Shinichi, Adhikari Rameshwar
Research Centre for Applied Science and Technology (RECAST), Tribhuvan University, Kirtipur, Kathmandu, Nepal.
Central Department of Chemistry, Tribhuvan University, Kirtipur, Kathmandu, Nepal.
Int J Biomater. 2020 Aug 28;2020:1690178. doi: 10.1155/2020/1690178. eCollection 2020.
A novel natural hydroxyapatite (HAp) bioceramic was extracted from the ostrich cortical bone by the thermal decomposition method. HAp was characterized by different analytical tools such as thermogravimetric analysis (TGA), Fourier-transform infrared spectroscopy (FTIR), X-ray diffraction (XRD) analysis, and scanning electron microscopy (SEM). Removal of organic impurities from the bone powder was confirmed by TGA analysis. FTIR spectra of HAp confirmed the presence of the major functional groups such as phosphate (PO ), hydroxyl (OH), and carbonate (CO ) in the bioceramic. The XRD data revealed that the HAp was the crystalline phase obtained by calcination of the bone powder at 950°C, and the SEM analyses confirmed the typical plate-like texture of the nanosized HAp crystals.
采用热分解法从鸵鸟皮质骨中提取了一种新型天然羟基磷灰石(HAp)生物陶瓷。通过热重分析(TGA)、傅里叶变换红外光谱(FTIR)、X射线衍射(XRD)分析和扫描电子显微镜(SEM)等不同分析工具对HAp进行了表征。通过TGA分析证实了从骨粉中去除了有机杂质。HAp的FTIR光谱证实了生物陶瓷中存在主要官能团,如磷酸盐(PO)、羟基(OH)和碳酸盐(CO)。XRD数据表明,HAp是通过在950°C下煅烧骨粉获得的晶相,SEM分析证实了纳米级HAp晶体具有典型的板状纹理。