García-Coronado Pedro, Flores-Ramírez Alma, Grajales-Lagunes Alicia, Godínez-Hernández Cesar, Abud-Archila Miguel, González-García Raúl, Ruiz-Cabrera Miguel A
Faculty of Chemical Sciences, Autonomous University of San Luis Potosí, Manuel Nava 6, San Luis Potosí 78290, Mexico.
Desert Zones Research Institute, Autonomous University of San Luis Potosí, Altair 200, San Luis Potosí 78377, Mexico.
Polymers (Basel). 2020 Sep 12;12(9):2077. doi: 10.3390/polym12092077.
The state diagram, which is defined as a stability map of different states and phases of a food as a function of the solid content and temperature, is regarded as fundamental approach in the design and optimization of processes or storage procedures of food in the low-, intermediate-, and high-moisture domains. Therefore, in this study, the effects of maltodextrin addition on the freezing points (Tm', Tm) and glass transition temperatures (Tg', Tg) required for the construction of state diagrams of fruit juice model systems by using differential scanning calorimetry methods was investigated. A D-optimal experimental design was used to prepare a total of 25 anhydrous model food systems at various dry mass fractions of fructose, glucose, sucrose, pectin, citric acid, and maltodextrin, in which this last component varied between 0 and 0.8. It was found that maltodextrin mass fractions higher than 0.4 are required to induce significant increases of Tg', Tm', Tg, and Tm curves. From this perspective, maltodextrin is a good alternative as a cryoprotectant and as a carrier agent in the food industry. Furthermore, solute-composition-based mathematical models were developed to evaluate the influence of the chemical composition on the thermal transitions and to predict the state diagrams of fruit juices at different maltodextrin mass fractions.
状态图被定义为食品不同状态和相作为固体含量和温度函数的稳定性图谱,被视为在低、中、高水分领域设计和优化食品加工或储存程序的基本方法。因此,在本研究中,采用差示扫描量热法研究了添加麦芽糊精对构建果汁模型系统状态图所需的冰点(Tm',Tm)和玻璃化转变温度(Tg',Tg)的影响。采用D-最优实验设计,在果糖、葡萄糖、蔗糖、果胶、柠檬酸和麦芽糊精的不同干质量分数下制备了总共25个无水模型食品体系,其中最后一种成分的含量在0到0.8之间变化。研究发现,需要高于0.4的麦芽糊精质量分数才能使Tg'、Tm'、Tg和Tm曲线显著增加。从这个角度来看,麦芽糊精作为食品工业中的冷冻保护剂和载体剂是一个很好的选择。此外,还开发了基于溶质组成的数学模型,以评估化学成分对热转变的影响,并预测不同麦芽糊精质量分数下果汁的状态图。